Which batches used AIBN catalyst?21 Aug 02:09
I have the answer. Batches 34–37, 39, 40 (plus the unlinked notebook note) all list AIBN catalyst.
Batches using AIBN catalyst (per the structured 9076 records):
Plus one unlinked record,
All are synthesis records where AIBN appears as
Note: the other document hits (EP 2115023 B1 patent, "9076 Exp 48-60", "LBN 34 -B", "Old ELN SummaryReport") are reference/other-doc text and are not the batch records that matched.
Batches using AIBN catalyst (per the structured 9076 records):
- Batch 34 (R-53/07032024) — AIBN 0.2 gm + 0.32 gm
- Batch 34 B
- Batch 34 C
- Batch 35
- Batch 36
- Batch 37
- Batch 37 A
- Batch 39
- Batch 40
Plus one unlinked record,
exp-9076-000UNKNOWNNOTEB ("notebook p19, step-1, Phosphate E3+2, Date 2021/1/26"), which also lists AIBN — this is a stub/unlinked notebook entry, not a confirmed numbered batch.All are synthesis records where AIBN appears as
role: "catalyst" in the step-2 material list. Batch 34 is the confirmed one: step 2 lists "iii) AIBN catalyst, 0.2 gm" and "v) AIBN catalyst, 0.32 gm" in toluene at 68-72 °C / N2 [28112025 9076 Expt Table 2025.xls, sheet 9076_Experiments, batch block '34'].Note: the other document hits (EP 2115023 B1 patent, "9076 Exp 48-60", "LBN 34 -B", "Old ELN SummaryReport") are reference/other-doc text and are not the batch records that matched.
Sources
find --material AIBN matches: exp-9076-034, 034B, 034C, 035, 036, 037, 037A, 039, 040, and 000UNKNOWNNOTEB
confidence: high