What equipment was used in batch 10?21 Aug 01:32
The ELN's "Equipment Details" field has the answer. It's page 1 of the PDF (OCR
Equipment for batch 10 (Lab Batch 10, date 19.05.23):
The structured record (exp-9076-010) does not carry a dedicated equipment field, but the linked ELN report does. The "Equipment Details" row reads verbatim:
> "Laboratory glass reactor set up with agitator / nitrogen system etc."
So the equipment was a laboratory glass reactor, set up with an agitator and a nitrogen (N₂) system (plus related ancillaries, as noted by "etc."). This is consistent with the process steps, which all run under stirring and nitrogen atmosphere ("main reactor ... under stirring and nitrogen atmosphere") — Step A at 60–75 °C, Step B at 55–80 °C, Step C at 55–65 °C [Lab Batch 10.pdf, page 1].
Note: no specific reactor size/model or instrument make is given in the record or the ELN — only this general "glass reactor + agitator + nitrogen system" description. That is the full extent of what the data drop contains on equipment.
_0 = page 1).Equipment for batch 10 (Lab Batch 10, date 19.05.23):
The structured record (exp-9076-010) does not carry a dedicated equipment field, but the linked ELN report does. The "Equipment Details" row reads verbatim:
> "Laboratory glass reactor set up with agitator / nitrogen system etc."
So the equipment was a laboratory glass reactor, set up with an agitator and a nitrogen (N₂) system (plus related ancillaries, as noted by "etc."). This is consistent with the process steps, which all run under stirring and nitrogen atmosphere ("main reactor ... under stirring and nitrogen atmosphere") — Step A at 60–75 °C, Step B at 55–80 °C, Step C at 55–65 °C [Lab Batch 10.pdf, page 1].
Note: no specific reactor size/model or instrument make is given in the record or the ELN — only this general "glass reactor + agitator + nitrogen system" description. That is the full extent of what the data drop contains on equipment.
Sources
confidence: high