Experiments / Batch 5
Batch 5 OK
27.12.22 ·
also written as Lab Batch 05 · S 399 #B 5 · S 9076 #L05 · S 9076 #L05B · 5
Conclusion — verbatim from the source
“Product was Yellowish flow able liquid/ Tested on different pigment found equivalent results to reference product/ Only re solubility parameters was inferior etc.”
pdf/9076 Data for Raven POC project/Old ELN/Lab Batch 05.pdf, page 2
Aim
To develop product equivalent to reference product
Observations
Appearance was yellowish with slight gripped in viscosity (Step-A) slowly gripped in viscosity found (Step-B) Yellowish flow able liquid (Step-B remarks) Expt Table remarks: Exotherm found while feed , moderate viscosity
Raw materials
| # | Material | Source | Qty | Purity % |
|---|---|---|---|---|
| 1 | Vicasurf -1010 | FOIL | 300 gms | 100 |
| 2 | Phosphorous pentaoxide | FOIL | 10.5 gms | 100 |
| 3 | Lupasol G-20 WF | FOIL | 7.5 gms | 100 |
Reaction conditions (optimized)
atmosphere: nitrogen
Process
| Step | Conditions | Charged | What happened | Results | ||||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
|
Step 1
Step A
28112025 9076 Expt Table 2025.xls · Lab Batch 05.pdf
|
temperature: 40 / 55 / 75 °Catmosphere: N2time: 0.15 / 0.5 / 1 hr-2 hr · ELN: 1-5 h |
Vicasurf -1010 300 g Phosphorous pentaoxide 10.5 g (Table: 10.2 g)
|
Step- A To main reactor added Vicasurf 1010 under stirring and nitrogen atmosphere temp. 40 deg increased temp slowly with addition of P- pentaoxide. Upon feed completion temp raised to 75 deg C and digested for 2-3 hrs. Appearance was yellowish with slight gripped in viscosity. Upon digestion cooled to RT. [ELN]
Exotherm found while feed , moderate viscosity [Table]
Step-by-step (3 entries)
|
acid_value 38 | ||||||||||||||||
|
Step 2
Step B
28112025 9076 Expt Table 2025.xls · Lab Batch 05.pdf
|
temperature: 40 / 70 °Catmosphere: N2time: 0.5 / 2 h · ELN: 1-3 h |
Step- 1 product 152 g Lupasol G-20 WF 7.5 g
|
Step-B To main reactor added Step- A reaction mass under stirring and nitrogen atmosphere temp. 40 deg Started slowly addition of Lupasol G-20 WF slowly , slowly gripped in viscosity found. upon feed completion stirred well for 1-2 hrs then cooled to RT. [ELN]
Yellowish flow able liquid [ELN remarks]
Step-by-step (2 entries)
|
acid_value 38amine_value 19 |
Critical parameters — measured vs target
| Parameter | Target | Measured |
|---|---|---|
| aminev | 30.1 | |
| av | 43.2 |
Sample S 399 #B 5
result
Violet 23 (NC-PU ink)
| Parameter | This sample | Standard (BYK 9076 Standard) |
|---|---|---|
| Viscosity | 36 sec | 35 sec |
| Gloss | 65.6 | 70.6 |
| Colour Strength | 1 | 1 |
| Resolubility | 5 | 4 |
| Transparency | Eq. to Std | Ref as Std |
APP DATA- BYK 9076 equivalent.xlsx
result
Black (NC-PU ink)
| Parameter | This sample | Standard (BYK 9076 Standard) |
|---|---|---|
| Viscosity | 38 sec | 36 sec |
| Gloss | 37 | 35.3 |
| Colour Strength | 1 | 1 |
| Resolubility | 5 | 4 |
| Transparency | Eq to Std | Ref as Std |
APP DATA- BYK 9076 equivalent.xlsx
Sample S 9076 #L05
result
Violet 23 (NC-PU ink)
| Parameter | This sample | Standard (BYK 9076 Standard) |
|---|---|---|
| Viscosity | 38 sec | 37 sec |
| Gloss | 54.6 | 53.9 |
| Colour Strength | 1 | 1 |
| Resolubility | 4 | 4 |
| Transparency | Eq. to Std | Ref as Std |
APP DATA- BYK 9076 equivalent.xlsx
result
Violet 27 (NC-PU ink)
| Parameter | This sample | Standard (BYK 9076 Standard) |
|---|---|---|
| Viscosity | 40 sec | 34 sec |
| Gloss | 8.8 | 7.2 |
| Colour Strength | 1 | 1 |
| Resolubility | 4 | 4 |
| Transparency | Eq to std | Ref as Std |
APP DATA- BYK 9076 equivalent.xlsx
result
Black (NC-PU ink)
| Parameter | This sample | Standard (BYK 9076 Standard) |
|---|---|---|
| Viscosity | 35 sec | 28 sec |
| Gloss | 20.9 | 41.5 |
| Colour Strength | 80 - 90% | 1 |
| Resolubility | 4 | 4 |
| Transparency | Eq to Std | Ref as Std |
APP DATA- BYK 9076 equivalent.xlsx
Sample S 9076 #L05B
result
Violet 23 (NC-PU ink)
| Parameter | This sample | Standard (BYK 9076 Standard) |
|---|---|---|
| Viscosity | 38 sec | 37 sec |
| Gloss | 54.6 | 53.9 |
| Colour Strength | 1 | 1 |
| Resolubility | 4 | 4 |
| Transparency | Eq. to Std | Ref as Std |
APP DATA- BYK 9076 equivalent.xlsx
result
Violet 27 (NC-PU ink)
| Parameter | This sample | Standard (BYK 9076 Standard) |
|---|---|---|
| Viscosity | 40 sec | 40 sec |
| Gloss | 8.8 | 7.2 |
| Colour Strength | 1 | 1 |
| Resolubility | 4 | 4 |
| Transparency | Eq to std | Ref as Std |
APP DATA- BYK 9076 equivalent.xlsx
result
Black (NC-PU ink)
| Parameter | This sample | Standard (BYK 9076 Standard) |
|---|---|---|
| Viscosity | 36 sec | 28 sec |
| Gloss | 28.4 | 41.5 |
| Colour Strength | 80 - 90% | 1 |
| Resolubility | 4 | 4 |
| Transparency | Eq to Std | Ref as Std |
APP DATA- BYK 9076 equivalent.xlsx
Where this record comes from
Lab Batch 05.pdf
— lab journal (primary source)
APP DATA- BYK 9076 equivalent.xlsx
— application testing · linked by a person
28112025 9076 Expt Table 2025.xls
— researcher summary (cross-check)
Something wrong on this page? Record a correction
Your correction is permanent: it survives every re-extraction and the field can no longer be changed by the system.
Field-by-field provenance (19 fields) — for auditors
5 extraction fragments · merged 2026-08-25 · 0 human-validated fields
Fix a wrong or missing extraction side-by-side with the original:
qwen-extract--lab-batch-05--lab-batch-05
app-data--S 399 #B 5
app-data--S 9076 #L05
app-data--S 9076 #L05B
expt-block--5
| Field | Source | Extractor | Conf. |
|---|---|---|---|
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| aim | Lab Batch 05.pdf page 1 (all tables), page 2 (Conclusion block) | qwen-tasks/extract-fragment.md@unversioned | high |
| conclusion | Lab Batch 05.pdf page 1 (all tables), page 2 (Conclusion block) | qwen-tasks/extract-fragment.md@unversioned | high |
| conditions.atmosphere | Lab Batch 05.pdf page 1 (all tables), page 2 (Conclusion block) | qwen-tasks/extract-fragment.md@unversioned | high |
| materials[0] | Lab Batch 05.pdf page 1 (all tables), page 2 (Conclusion block) | qwen-tasks/extract-fragment.md@unversioned | high |
| materials[1] | Lab Batch 05.pdf page 1 (all tables), page 2 (Conclusion block) | qwen-tasks/extract-fragment.md@unversioned | high |
| materials[2] | Lab Batch 05.pdf page 1 (all tables), page 2 (Conclusion block) | qwen-tasks/extract-fragment.md@unversioned | high |
| process_steps[0] | Lab Batch 05.pdf page 1 (all tables), page 2 (Conclusion block) | qwen-tasks/extract-fragment.md@unversioned | high |
| process_steps[1] | Lab Batch 05.pdf page 1 (all tables), page 2 (Conclusion block) | qwen-tasks/extract-fragment.md@unversioned | high |
| critical_parameters[0] | Lab Batch 05.pdf page 1 (all tables), page 2 (Conclusion block) | qwen-tasks/extract-fragment.md@unversioned | high |
| critical_parameters[1] | Lab Batch 05.pdf page 1 (all tables), page 2 (Conclusion block) | qwen-tasks/extract-fragment.md@unversioned | high |
| observations | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '5', csv rows 17-20 | qwen-tasks/extract-expt-block.md@unversioned | high |
| outcome | Lab Batch 05.pdf page 1 (all tables), page 2 (Conclusion block) | qwen-tasks/extract-fragment.md@unversioned | high |
| samples[0] | APP DATA- BYK 9076 equivalent.xlsx sheet BYK_9076_equivalent, rows 39-39 | parse_app_data.py@unversioned | high |
| samples[1] | APP DATA- BYK 9076 equivalent.xlsx sheet BYK_9076_equivalent, rows 66-66 | parse_app_data.py@unversioned | high |
| samples[2] | APP DATA- BYK 9076 equivalent.xlsx sheet BYK_9076_equivalent, rows 64-64 | parse_app_data.py@unversioned | high |
| record_type | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '5', csv rows 17-20 | qwen-tasks/extract-expt-block.md@unversioned | high |
| process_steps[2] | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '5', csv rows 17-20 | qwen-tasks/extract-expt-block.md@unversioned | high |
| process_steps[3] | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '5', csv rows 17-20 | qwen-tasks/extract-expt-block.md@unversioned | high |
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"date": "27.12.22",
"aim": "To develop product equivalent to reference product",
"conclusion": "Product was Yellowish flow able liquid/ Tested on different pigment found equivalent results to reference product/ Only re solubility parameters was inferior etc.",
"conditions": {
"atmosphere": "nitrogen"
},
"materials": [
{
"sr_no": "1",
"name": "Vicasurf -1010",
"source": "FOIL",
"quantity": "300",
"unit": "gms",
"purity_pct": "100"
},
{
"sr_no": "2",
"name": "Phosphorous pentaoxide",
"source": "FOIL",
"quantity": "10.5",
"unit": "gms",
"purity_pct": "100"
},
{
"sr_no": "3",
"name": "Lupasol G-20 WF",
"source": "FOIL",
"quantity": "7.5",
"unit": "gms",
"purity_pct": "100"
}
],
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"time_hrs": "1-5",
"temperature": "40-75",
"temperature_unit": "°C",
"pressure_vacuum_n2": "Yes",
"procedure": [
{
"action": "Step- A To main reactor added Vicasurf 1010 under stirring and nitrogen atmosphere temp. 40 deg increased temp slowly with addition of P- pentaoxide . Upon feed completion temp raised to 75 deg C and digested for 2-3 hrs. Appearance was yellowish with slight gripped in viscosity. Upon digestion cooled to RT.AV-38"
}
],
"results": [
{
"measurement": "AV",
"value": "38",
"verbatim": "AV-38",
"parameter": "unlabelled"
}
]
},
{
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"time_hrs": "1-3",
"temperature": "40-70",
"temperature_unit": "°C",
"pressure_vacuum_n2": "Yes",
"procedure": [
{
"action": "Step-B To main reactor added Step- A reaction mass under stirring and nitrogen atmosphere temp. 40 deg Started slowly addition of Lupasol G-20 WF slowly , slowly gripped in viscosity found. upon feed completion stirred well for 1-2 hrs then cooled to RT.AV-38 Amine Value- 19"
}
],
"remarks": "Yellowish flow able liquid",
"results": [
{
"measurement": "AV",
"value": "38",
"verbatim": "AV-38",
"parameter": "unlabelled"
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{
"measurement": "Amine Value",
"value": "19",
"verbatim": "Amine Value- 19",
"parameter": "unlabelled"
}
]
},
{
"step": 1,
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"quantity": 300,
"unit": "g",
"role": "reactant"
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{
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"quantity": 10.2,
"unit": "g",
"role": "reactant"
}
],
"procedure": [
{
"seq": 1,
"temperature": "40",
"time_h": "0.15",
"action": "Ramp stage 1",
"observation": "Exotherm found while feed , moderate viscosity"
},
{
"seq": 2,
"temperature": "55",
"time_h": "0.5",
"atmosphere": "N2",
"action": "Ramp stage 2"
},
{
"seq": 3,
"temperature": "75",
"time_h": "1 hr-2 hr",
"action": "Ramp stage 3"
}
],
"conditions": {
"temperature": "40 / 55 / 75",
"atmosphere": "N2",
"time_h": "0.15 / 0.5 / 1 hr-2 hr"
},
"results": [
{
"parameter": "A.V.",
"value": 38,
"phase": "final",
"verbatim": "38"
}
],
"remarks": "Exotherm found while feed , moderate viscosity"
},
{
"step": 2,
"materials": [
{
"name": "Step- 1 product",
"quantity": 152,
"unit": "g",
"role": "intermediate"
},
{
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"quantity": 7.5,
"unit": "g",
"role": "reactant"
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],
"procedure": [
{
"seq": 1,
"temperature": "40",
"time_h": "0.5",
"atmosphere": "N2",
"action": "Ramp stage 1"
},
{
"seq": 2,
"temperature": "70",
"time_h": "2",
"action": "Ramp stage 2"
}
],
"conditions": {
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"atmosphere": "N2",
"time_h": "0.5 / 2"
},
"results": [
{
"parameter": "A.V.",
"value": 38,
"phase": "final",
"verbatim": "AV-38"
},
{
"parameter": "amine value",
"value": 19,
"phase": "final",
"verbatim": "Amine value- 19"
}
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}
],
"critical_parameters": [
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"parameter": "aminev",
"reference_value": "30.1"
},
{
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"parameter": "av",
"reference_value": "43.2"
}
],
"observations": "Appearance was yellowish with slight gripped in viscosity (Step-A)\nslowly gripped in viscosity found (Step-B)\nYellowish flow able liquid (Step-B remarks)\n\nExpt Table remarks: Exotherm found while feed , moderate viscosity",
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{
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"application_tests": [
{
"test": "Violet 23",
"system": "NC-PU ink",
"conditions": "trial 05.12.2025",
"result": "Viscosity: 36 sec; Gloss: 65.6; Colour Strength: 1; Resolubility: 5; Transparency: Eq. to Std",
"vs_reference": "BYK 9076 Standard — Viscosity: 35 sec; Gloss: 70.6; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
"file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
},
{
"test": "Black",
"system": "NC-PU ink",
"conditions": "trial 05.12.2025",
"result": "Viscosity: 38 sec; Gloss: 37; Colour Strength: 1; Resolubility: 5; Transparency: Eq to Std",
"vs_reference": "BYK 9076 Standard — Viscosity: 36 sec; Gloss: 35.3; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
"file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
}
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},
{
"sample_id": "S 9076 #L05",
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{
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"system": "NC-PU ink",
"conditions": "trial 05.02.2025",
"result": "Viscosity: 38 sec; Gloss: 54.6; Colour Strength: 1; Resolubility: 4; Transparency: Eq. to Std",
"vs_reference": "BYK 9076 Standard — Viscosity: 37 sec; Gloss: 53.9; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
"file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
},
{
"test": "Violet 27",
"system": "NC-PU ink",
"conditions": "trial 05.02.2025",
"result": "Viscosity: 40 sec; Gloss: 8.8; Colour Strength: 1; Resolubility: 4; Transparency: Eq to std",
"vs_reference": "BYK 9076 Standard — Viscosity: 34 sec; Gloss: 7.2; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
"file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
},
{
"test": "Black",
"system": "NC-PU ink",
"conditions": "trial 05.02.2025",
"result": "Viscosity: 35 sec; Gloss: 20.9; Colour Strength: 80 - 90%; Resolubility: 4; Transparency: Eq to Std",
"vs_reference": "BYK 9076 Standard — Viscosity: 28 sec; Gloss: 41.5; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
"file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
}
]
},
{
"sample_id": "S 9076 #L05B",
"application_tests": [
{
"test": "Violet 23",
"system": "NC-PU ink",
"conditions": "trial 07.02.2025",
"result": "Viscosity: 38 sec; Gloss: 54.6; Colour Strength: 1; Resolubility: 4; Transparency: Eq. to Std",
"vs_reference": "BYK 9076 Standard — Viscosity: 37 sec; Gloss: 53.9; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
"file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
},
{
"test": "Violet 27",
"system": "NC-PU ink",
"conditions": "trial 07.02.2025",
"result": "Viscosity: 40 sec; Gloss: 8.8; Colour Strength: 1; Resolubility: 4; Transparency: Eq to std",
"vs_reference": "BYK 9076 Standard — Viscosity: 40 sec; Gloss: 7.2; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
"file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
},
{
"test": "Black",
"system": "NC-PU ink",
"conditions": "trial 07.02.2025",
"result": "Viscosity: 36 sec; Gloss: 28.4; Colour Strength: 80 - 90%; Resolubility: 4; Transparency: Eq to Std",
"vs_reference": "BYK 9076 Standard — Viscosity: 28 sec; Gloss: 41.5; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
"file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
}
]
}
],
"record_type": "synthesis"
}