Observations
Expt Table remarks: For Carbon black pigment-Gloss, Tinting strength, Shade good having adhesion dots while cleaning Ink removal Batch 2=3<4<5
Raw materials (collected from the per-step charges)
| Step | Material | Qty | Role |
|---|---|---|---|
| 1 | Vicasurf -1010 | 250 g | reactant |
| 1 | Butanol- 2 EO-2PO | 50 g | reactant |
| 1 | Phosphorous pentaoxide | 15 g | reactant |
| 2 | Step- 1 product | 150 g | intermediate |
| 2 | Lupasol G-20 WF | 13.5 g | reactant |
Process
| Step | Conditions | Charged | What happened | Results |
|---|---|---|---|---|
|
Step 1
28112025 9076 Expt Table 2025.xls
|
temperature: 40 / 55 / 75atmosphere: N2time_h: 0.15 / 0.5 / 1 hr-2 hr |
Vicasurf -1010 250g Butanol- 2 EO-2PO 50g Phosphorous pentaoxide 15g
|
During feeding found slight exotherm ,
slight grip in viscosity with distinct turbidity( Not like sunflower oil)
—
|
A.V. 53 |
|
Step 2
28112025 9076 Expt Table 2025.xls
|
temperature: 45 / 65atmosphere: N2time_h: 0.5 / 2.5 |
Step- 1 product 150g Lupasol G-20 WF 13.5g
|
— | A.V. 53 amine value 42 |
Sample S 9076 #RSB04-A
result
Violet 23 (NC-PU ink)
| Parameter | This sample | Standard (BYK 9076 Standard) |
|---|---|---|
| Viscosity | 33 sec | 29 sec |
| Gloss | 53.8 | 65.1 |
| Colour Strength | 97 - 98.00% | 1 |
| Resolubility | 4 | 4 |
| Transparency | Opaque | Ref as Std |
APP DATA- BYK 9076 equivalent.xlsx
result
Black (NC-PU ink)
| Parameter | This sample | Standard (BYK 9076 Standard) |
|---|---|---|
| Viscosity | 47 sec | 46 sec |
| Gloss | 39.8 | 41.3 |
| Colour Strength | 1 | 1 |
| Resolubility | 5 | 4 |
| Transparency | Eq to Std | Ref as Std |
APP DATA- BYK 9076 equivalent.xlsx
Where this record comes from
APP DATA- BYK 9076 equivalent.xlsx
— application testing · linked by a person
28112025 9076 Expt Table 2025.xls
— researcher summary (cross-check)
Something wrong on this page? Record a correction
Your correction is permanent: it survives every re-extraction and the field can no longer be changed by the system.
Field-by-field provenance (5 fields) — for auditors
2 extraction fragments · merged 2026-08-25 · 0 human-validated fields
Fix a wrong or missing extraction side-by-side with the original:
app-data--S 9076 #RSB04-A
expt-block--4
| Field | Source | Extractor | Conf. |
|---|---|---|---|
| samples[0] | APP DATA- BYK 9076 equivalent.xlsx sheet BYK_9076_equivalent, rows 31-31 | parse_app_data.py@unversioned | high |
| record_type | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '4', csv rows 13-16 | qwen-tasks/extract-expt-block.md@unversioned | high |
| process_steps[0] | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '4', csv rows 13-16 | qwen-tasks/extract-expt-block.md@unversioned | high |
| process_steps[1] | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '4', csv rows 13-16 | qwen-tasks/extract-expt-block.md@unversioned | high |
| observations | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '4', csv rows 13-16 | qwen-tasks/extract-expt-block.md@unversioned | high |
Raw record JSON
{
"record_id": "exp-9076-004",
"project": "9076",
"aliases": [
"S 9076 #RSB04-A",
"4"
],
"provenance": {
"fragments": [
"app-data--S 9076 #RSB04-A",
"expt-block--4"
],
"field_provenance": {
"samples[0]": {
"source_file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx",
"extractor": "parse_app_data.py",
"extractor_version": "unversioned",
"extracted_date": "2026-08-19",
"locator": "sheet BYK_9076_equivalent, rows 31-31",
"human_checked": true
},
"record_type": {
"source_file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"extractor": "qwen-tasks/extract-expt-block.md",
"extractor_version": "unversioned",
"extracted_date": "2026-08-19",
"locator": "sheet 9076_Experiments, batch block '4', csv rows 13-16",
"human_checked": true
},
"process_steps[0]": {
"source_file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"extractor": "qwen-tasks/extract-expt-block.md",
"extractor_version": "unversioned",
"extracted_date": "2026-08-19",
"locator": "sheet 9076_Experiments, batch block '4', csv rows 13-16",
"human_checked": true
},
"process_steps[1]": {
"source_file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"extractor": "qwen-tasks/extract-expt-block.md",
"extractor_version": "unversioned",
"extracted_date": "2026-08-19",
"locator": "sheet 9076_Experiments, batch block '4', csv rows 13-16",
"human_checked": true
},
"observations": {
"source_file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"extractor": "qwen-tasks/extract-expt-block.md",
"extractor_version": "unversioned",
"extracted_date": "2026-08-19",
"locator": "sheet 9076_Experiments, batch block '4', csv rows 13-16",
"human_checked": true
}
},
"last_merged": "2026-08-25"
},
"documents": [
{
"file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx",
"role": "application_test",
"link_basis": "human link (exp-9076-004)",
"link_status": "user-confirmed"
},
{
"file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"role": "summary_table",
"link_basis": "alias match: 4",
"link_status": "rule"
}
],
"validation": {
"validated_fields": {},
"corrections_applied": []
},
"samples": [
{
"sample_id": "S 9076 #RSB04-A",
"application_tests": [
{
"test": "Violet 23",
"system": "NC-PU ink",
"conditions": "trial 17.12.2025",
"result": "Viscosity: 33 sec; Gloss: 53.8; Colour Strength: 97 - 98.00%; Resolubility: 4; Transparency: Opaque",
"vs_reference": "BYK 9076 Standard — Viscosity: 29 sec; Gloss: 65.1; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
"file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
},
{
"test": "Black",
"system": "NC-PU ink",
"conditions": "trial 17.12.2025",
"result": "Viscosity: 47 sec; Gloss: 39.8; Colour Strength: 1; Resolubility: 5; Transparency: Eq to Std",
"vs_reference": "BYK 9076 Standard — Viscosity: 46 sec; Gloss: 41.3; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
"file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
}
]
}
],
"record_type": "synthesis",
"process_steps": [
{
"step": 1,
"materials": [
{
"name": "Vicasurf -1010",
"quantity": 250,
"unit": "g",
"role": "reactant"
},
{
"name": "Butanol- 2 EO-2PO",
"quantity": 50,
"unit": "g",
"role": "reactant"
},
{
"name": "Phosphorous pentaoxide",
"quantity": 15,
"unit": "g",
"role": "reactant"
}
],
"procedure": [
{
"seq": 1,
"temperature": "40",
"time_h": "0.15",
"atmosphere": "N2",
"action": "Ramp stage 1",
"observation": "During feeding found slight exotherm ,\nslight grip in viscosity with distinct turbidity( Not like sunflower oil)"
},
{
"seq": 2,
"temperature": "55",
"time_h": "0.5",
"atmosphere": "N2",
"action": "Ramp stage 2"
},
{
"seq": 3,
"temperature": "75",
"time_h": "1 hr-2 hr",
"atmosphere": "N2",
"action": "Ramp stage 3"
}
],
"conditions": {
"temperature": "40 / 55 / 75",
"atmosphere": "N2",
"time_h": "0.15 / 0.5 / 1 hr-2 hr"
},
"results": [
{
"parameter": "A.V.",
"value": 53,
"phase": "final",
"verbatim": "53"
}
],
"remarks": "During feeding found slight exotherm ,\nslight grip in viscosity with distinct turbidity( Not like sunflower oil)"
},
{
"step": 2,
"materials": [
{
"name": "Step- 1 product",
"quantity": 150,
"unit": "g",
"role": "intermediate"
},
{
"name": "Lupasol G-20 WF",
"quantity": 13.5,
"unit": "g",
"role": "reactant"
}
],
"procedure": [
{
"seq": 1,
"temperature": "45",
"time_h": "0.5",
"atmosphere": "N2",
"action": "Ramp stage 1"
},
{
"seq": 2,
"temperature": "65",
"time_h": "2.5",
"atmosphere": "N2",
"action": "Ramp stage 2"
}
],
"conditions": {
"temperature": "45 / 65",
"atmosphere": "N2",
"time_h": "0.5 / 2.5"
},
"results": [
{
"parameter": "A.V.",
"value": 53,
"phase": "final",
"verbatim": "AV-53"
},
{
"parameter": "amine value",
"value": 42,
"phase": "final",
"verbatim": "Amine value-42"
}
]
}
],
"observations": "Expt Table remarks: For Carbon black pigment-Gloss, Tinting strength, Shade good \nhaving adhesion dots while cleaning Ink removal Batch 2=3<4<5"
}