Batch 3 — Raven Records

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Experiments / Batch 3

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also written as S 9076 #L03 · S 9076 #L03A · S 9076 #L03B · S 9076 #L03C · S 9076 #L03D · S 9076 #L03E · 3

Observations

Expt Table remarks: During feeding found slight exotherm , Very fine yellow tincture found , slight grip in viscosity found

Raw materials (collected from the per-step charges)

Step	Material	Qty	Role
1	MPEG-350	150 g	reactant
1	Tripropylene glycol mono-butyl ether	150 g	reactant
1	Phosphorous pentaoxide	13.2 g	reactant
2	Step- 1 product	152 g	intermediate
2	Lupasol G-20 WF	13.8 g	reactant

Process

Step	Conditions	Charged	What happened	Results
Step 1 28112025 9076 Expt Table 2025.xls	temperature: 35 / 55 / 60atmosphere: N2time_h: 0.15 / 1 / 2	MPEG-350 150g Tripropylene glycol mono-butyl ether 150g Phosphorous pentaoxide 13.2g	During feeding found slight exotherm , Very fine yellow tincture found , slight grip in viscosity found —	A.V. 55
Step 2 28112025 9076 Expt Table 2025.xls	temperature: 40 / 65atmosphere: N2time_h: 0.5 / 2	Step- 1 product 152g Lupasol G-20 WF 13.8g	—	A.V. 48 amine value 42

Step 1

temperature: 35 / 55 / 60atmosphere: N2time_h: 0.15 / 1 / 2

Charged: MPEG-350 150g · Tripropylene glycol mono-butyl ether 150g · Phosphorous pentaoxide 13.2g

A.V. 55

Step-by-step (3 entries)

Time (h)	Temp (°C)	Atmosphere	What happened
0.15	35	N2	Ramp stage 1 During feeding found slight exotherm , Very fine yellow tincture found , slight grip in viscosity found
1	55	N2	Ramp stage 2
2	60	N2	Ramp stage 3

During feeding found slight exotherm , Very fine yellow tincture found , slight grip in viscosity found

Step 2

temperature: 40 / 65atmosphere: N2time_h: 0.5 / 2

Charged: Step- 1 product 152g · Lupasol G-20 WF 13.8g

A.V. 48 amine value 42

Step-by-step (2 entries)

Time (h)	Temp (°C)	Atmosphere	What happened
0.5	40	N2	Ramp stage 1
2	65	N2	Ramp stage 2

Sample S 9076 #L03

result Violet 27 (NC-PU ink)

Parameter	This sample	Standard (BYK 9076 Standard)
Viscosity	40 sec	39 sec
Gloss	7.2	6.6
Colour Strength	1	1
Resolubility	2	4
Transparency	Slightly redder	Ref as Std

APP DATA- BYK 9076 equivalent.xlsx

Sample S 9076 #L03A

result Violet 23 (NC-PU ink)

Parameter	This sample	Standard (BYK 9076 Standard)
Viscosity	36 sec	35 sec
Gloss	59.8	56.7
Colour Strength	1	1
Resolubility	4	4
Transparency	Eq. to Std	Ref as Std

APP DATA- BYK 9076 equivalent.xlsx

result Violet 27 (NC-PU ink)

Parameter	This sample	Standard (BYK 9076 Standard)
Viscosity	40 sec	39 sec
Gloss	7.3	7
Colour Strength	97 - 98%	1
Resolubility	4	4
Transparency	Slightly redder	Ref as Std

APP DATA- BYK 9076 equivalent.xlsx

Sample S 9076 #L03B

result Violet 23 (NC-PU ink)

Parameter	This sample	Standard (BYK 9076 Standard)
Viscosity	37 sec	35 sec
Gloss	60.4	56.7
Colour Strength	1	1
Resolubility	4	4
Transparency	Eq. to Std	Ref as Std

APP DATA- BYK 9076 equivalent.xlsx

result Violet 27 (NC-PU ink)

Parameter	This sample	Standard (BYK 9076 Standard)
Viscosity	41 sec	39 sec
Gloss	7.6	7
Colour Strength	95 - 96.00%	1
Resolubility	2	4
Transparency	Slightly redder	Ref as Std

APP DATA- BYK 9076 equivalent.xlsx

Sample S 9076 #L03C

result Violet 23 (NC-PU ink)

Parameter	This sample	Standard (BYK 9076 Standard)
Viscosity	36 sec	35 sec
Gloss	57.9	56.1
Colour Strength	1	1
Resolubility	4	4
Transparency	Eq. to Std	Ref as Std

APP DATA- BYK 9076 equivalent.xlsx

result Violet 27 (NC-PU ink)

Parameter	This sample	Standard (BYK 9076 Standard)
Viscosity	40 sec	39 sec
Gloss	7.9	7.2
Colour Strength	1	1
Resolubility	2	4
Transparency	Eq. to Std	Ref as Std

APP DATA- BYK 9076 equivalent.xlsx

Sample S 9076 #L03D

result Violet 23 (NC-PU ink)

Parameter	This sample	Standard (BYK 9076 Standard)
Viscosity	35 sec	34 sec
Gloss	57.5	55.7
Colour Strength	1	1
Resolubility	4	4
Transparency	Eq. to Std	Ref as Std

APP DATA- BYK 9076 equivalent.xlsx

result Violet 27 (NC-PU ink)

Parameter	This sample	Standard (BYK 9076 Standard)
Viscosity	39 sec	39 sec
Gloss	7.6	7
Colour Strength	1	1
Resolubility	2	4
Transparency	Eq. to Std	Ref as Std

APP DATA- BYK 9076 equivalent.xlsx

Sample S 9076 #L03E

result Violet 27 (NC-PU ink)

Parameter	This sample	Standard (BYK 9076 Standard)
Viscosity	40 sec	39 sec
Gloss	7.8	7.2
Colour Strength	1	1
Resolubility	2	4
Transparency	Eq to std	Ref as Std

APP DATA- BYK 9076 equivalent.xlsx

Where this record comes from

APP DATA- BYK 9076 equivalent.xlsx — application testing · linked by a person

28112025 9076 Expt Table 2025.xls — researcher summary (cross-check)

Something wrong on this page? Record a correction

Your correction is permanent: it survives every re-extraction and the field can no longer be changed by the system.

Field-by-field provenance (10 fields) — for auditors

7 extraction fragments · merged 2026-08-25 · 0 human-validated fields

Fix a wrong or missing extraction side-by-side with the original: app-data--S 9076 #L03 app-data--S 9076 #L03A app-data--S 9076 #L03B app-data--S 9076 #L03C app-data--S 9076 #L03D app-data--S 9076 #L03E expt-block--3

Field	Source	Extractor	Conf.
samples[0]	APP DATA- BYK 9076 equivalent.xlsx sheet BYK_9076_equivalent, rows 80-80	parse_app_data.py@unversioned	high
samples[1]	APP DATA- BYK 9076 equivalent.xlsx sheet BYK_9076_equivalent, rows 76-76	parse_app_data.py@unversioned	high
samples[2]	APP DATA- BYK 9076 equivalent.xlsx sheet BYK_9076_equivalent, rows 74-74	parse_app_data.py@unversioned	high
samples[3]	APP DATA- BYK 9076 equivalent.xlsx sheet BYK_9076_equivalent, rows 72-72	parse_app_data.py@unversioned	high
samples[4]	APP DATA- BYK 9076 equivalent.xlsx sheet BYK_9076_equivalent, rows 70-70	parse_app_data.py@unversioned	high
samples[5]	APP DATA- BYK 9076 equivalent.xlsx sheet BYK_9076_equivalent, rows 68-68	parse_app_data.py@unversioned	high
record_type	28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '3', csv rows 9-12	qwen-tasks/extract-expt-block.md@unversioned	high
process_steps[0]	28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '3', csv rows 9-12	qwen-tasks/extract-expt-block.md@unversioned	high
process_steps[1]	28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '3', csv rows 9-12	qwen-tasks/extract-expt-block.md@unversioned	high
observations	28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '3', csv rows 9-12	qwen-tasks/extract-expt-block.md@unversioned	high

Raw record JSON

{
  "record_id": "exp-9076-003",
  "project": "9076",
  "aliases": [
    "S 9076 #L03",
    "S 9076 #L03A",
    "S 9076 #L03B",
    "S 9076 #L03C",
    "S 9076 #L03D",
    "S 9076 #L03E",
    "3"
  ],
  "provenance": {
    "fragments": [
      "app-data--S 9076 #L03",
      "app-data--S 9076 #L03A",
      "app-data--S 9076 #L03B",
      "app-data--S 9076 #L03C",
      "app-data--S 9076 #L03D",
      "app-data--S 9076 #L03E",
      "expt-block--3"
    ],
    "field_provenance": {
      "samples[0]": {
        "source_file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx",
        "extractor": "parse_app_data.py",
        "extractor_version": "unversioned",
        "extracted_date": "2026-08-19",
        "locator": "sheet BYK_9076_equivalent, rows 80-80",
        "human_checked": true
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      "samples[1]": {
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        "extracted_date": "2026-08-19",
        "locator": "sheet BYK_9076_equivalent, rows 76-76",
        "human_checked": true
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      "samples[2]": {
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        "extractor": "parse_app_data.py",
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        "locator": "sheet BYK_9076_equivalent, rows 74-74",
        "human_checked": true
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      "samples[3]": {
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        "extractor": "parse_app_data.py",
        "extractor_version": "unversioned",
        "extracted_date": "2026-08-19",
        "locator": "sheet BYK_9076_equivalent, rows 72-72",
        "human_checked": true
      },
      "samples[4]": {
        "source_file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx",
        "extractor": "parse_app_data.py",
        "extractor_version": "unversioned",
        "extracted_date": "2026-08-19",
        "locator": "sheet BYK_9076_equivalent, rows 70-70",
        "human_checked": true
      },
      "samples[5]": {
        "source_file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx",
        "extractor": "parse_app_data.py",
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        "extracted_date": "2026-08-19",
        "locator": "sheet BYK_9076_equivalent, rows 68-68",
        "human_checked": true
      },
      "record_type": {
        "source_file": "docs/Project Expt Report/28112025  9076 Expt Table 2025.xls",
        "extractor": "qwen-tasks/extract-expt-block.md",
        "extractor_version": "unversioned",
        "extracted_date": "2026-08-19",
        "locator": "sheet 9076_Experiments, batch block '3', csv rows 9-12",
        "human_checked": true
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      "process_steps[0]": {
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        "extracted_date": "2026-08-19",
        "locator": "sheet 9076_Experiments, batch block '3', csv rows 9-12",
        "human_checked": true
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      "process_steps[1]": {
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        "extractor": "qwen-tasks/extract-expt-block.md",
        "extractor_version": "unversioned",
        "extracted_date": "2026-08-19",
        "locator": "sheet 9076_Experiments, batch block '3', csv rows 9-12",
        "human_checked": true
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      "observations": {
        "source_file": "docs/Project Expt Report/28112025  9076 Expt Table 2025.xls",
        "extractor": "qwen-tasks/extract-expt-block.md",
        "extractor_version": "unversioned",
        "extracted_date": "2026-08-19",
        "locator": "sheet 9076_Experiments, batch block '3', csv rows 9-12",
        "human_checked": true
      }
    },
    "last_merged": "2026-08-25"
  },
  "documents": [
    {
      "file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx",
      "role": "application_test",
      "link_basis": "human link (exp-9076-003)",
      "link_status": "user-confirmed"
    },
    {
      "file": "docs/Project Expt Report/28112025  9076 Expt Table 2025.xls",
      "role": "summary_table",
      "link_basis": "alias match: 3",
      "link_status": "rule"
    }
  ],
  "validation": {
    "validated_fields": {},
    "corrections_applied": []
  },
  "samples": [
    {
      "sample_id": "S 9076 #L03",
      "application_tests": [
        {
          "test": "Violet 27",
          "system": "NC-PU ink",
          "conditions": "trial 13.01.2025",
          "result": "Viscosity: 40 sec; Gloss: 7.2; Colour Strength: 1; Resolubility: 2; Transparency: Slightly redder",
          "vs_reference": "BYK 9076 Standard — Viscosity: 39 sec; Gloss: 6.6; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
          "file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
        }
      ]
    },
    {
      "sample_id": "S 9076 #L03A",
      "application_tests": [
        {
          "test": "Violet 23",
          "system": "NC-PU ink",
          "conditions": "trial 29.01.2025",
          "result": "Viscosity: 36 sec; Gloss: 59.8; Colour Strength: 1; Resolubility: 4; Transparency: Eq. to Std",
          "vs_reference": "BYK 9076 Standard — Viscosity: 35 sec; Gloss: 56.7; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
          "file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
        },
        {
          "test": "Violet 27",
          "system": "NC-PU ink",
          "conditions": "trial 29.01.2025",
          "result": "Viscosity: 40 sec; Gloss: 7.3; Colour Strength: 97 - 98%; Resolubility: 4; Transparency: Slightly redder",
          "vs_reference": "BYK 9076 Standard — Viscosity: 39 sec; Gloss: 7; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
          "file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
        }
      ]
    },
    {
      "sample_id": "S 9076 #L03B",
      "application_tests": [
        {
          "test": "Violet 23",
          "system": "NC-PU ink",
          "conditions": "trial 29.01.2025",
          "result": "Viscosity: 37 sec; Gloss: 60.4; Colour Strength: 1; Resolubility: 4; Transparency: Eq. to Std",
          "vs_reference": "BYK 9076 Standard — Viscosity: 35 sec; Gloss: 56.7; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
          "file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
        },
        {
          "test": "Violet 27",
          "system": "NC-PU ink",
          "conditions": "trial 29.01.2025",
          "result": "Viscosity: 41 sec; Gloss: 7.6; Colour Strength: 95 - 96.00%; Resolubility: 2; Transparency: Slightly redder",
          "vs_reference": "BYK 9076 Standard — Viscosity: 39 sec; Gloss: 7; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
          "file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
        }
      ]
    },
    {
      "sample_id": "S 9076 #L03C",
      "application_tests": [
        {
          "test": "Violet 23",
          "system": "NC-PU ink",
          "conditions": "trial 30.01.2025",
          "result": "Viscosity: 36 sec; Gloss: 57.9; Colour Strength: 1; Resolubility: 4; Transparency: Eq. to Std",
          "vs_reference": "BYK 9076 Standard — Viscosity: 35 sec; Gloss: 56.1; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
          "file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
        },
        {
          "test": "Violet 27",
          "system": "NC-PU ink",
          "conditions": "trial 30.01.2025",
          "result": "Viscosity: 40 sec; Gloss: 7.9; Colour Strength: 1; Resolubility: 2; Transparency: Eq. to Std",
          "vs_reference": "BYK 9076 Standard — Viscosity: 39 sec; Gloss: 7.2; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
          "file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
        }
      ]
    },
    {
      "sample_id": "S 9076 #L03D",
      "application_tests": [
        {
          "test": "Violet 23",
          "system": "NC-PU ink",
          "conditions": "trial 31.01.2025",
          "result": "Viscosity: 35 sec; Gloss: 57.5; Colour Strength: 1; Resolubility: 4; Transparency: Eq. to Std",
          "vs_reference": "BYK 9076 Standard — Viscosity: 34 sec; Gloss: 55.7; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
          "file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
        },
        {
          "test": "Violet 27",
          "system": "NC-PU ink",
          "conditions": "trial 31.01.2025",
          "result": "Viscosity: 39 sec; Gloss: 7.6; Colour Strength: 1; Resolubility: 2; Transparency: Eq. to Std",
          "vs_reference": "BYK 9076 Standard — Viscosity: 39 sec; Gloss: 7; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
          "file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
        }
      ]
    },
    {
      "sample_id": "S 9076 #L03E",
      "application_tests": [
        {
          "test": "Violet 27",
          "system": "NC-PU ink",
          "conditions": "trial 01.02.2025",
          "result": "Viscosity: 40 sec; Gloss: 7.8; Colour Strength: 1; Resolubility: 2; Transparency: Eq to std",
          "vs_reference": "BYK 9076 Standard — Viscosity: 39 sec; Gloss: 7.2; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
          "file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
        }
      ]
    }
  ],
  "record_type": "synthesis",
  "process_steps": [
    {
      "step": 1,
      "materials": [
        {
          "name": "MPEG-350",
          "quantity": 150,
          "unit": "g",
          "role": "reactant"
        },
        {
          "name": "Tripropylene glycol mono-butyl ether",
          "quantity": 150,
          "unit": "g",
          "role": "reactant"
        },
        {
          "name": "Phosphorous pentaoxide",
          "quantity": 13.2,
          "unit": "g",
          "role": "reactant"
        }
      ],
      "procedure": [
        {
          "seq": 1,
          "temperature": "35",
          "time_h": "0.15",
          "atmosphere": "N2",
          "action": "Ramp stage 1",
          "observation": "During feeding  found slight exotherm ,\nVery fine yellow tincture found , slight grip in viscosity found"
        },
        {
          "seq": 2,
          "temperature": "55",
          "time_h": "1",
          "atmosphere": "N2",
          "action": "Ramp stage 2"
        },
        {
          "seq": 3,
          "temperature": "60",
          "time_h": "2",
          "atmosphere": "N2",
          "action": "Ramp stage 3"
        }
      ],
      "conditions": {
        "temperature": "35 / 55 / 60",
        "atmosphere": "N2",
        "time_h": "0.15 / 1 / 2"
      },
      "results": [
        {
          "parameter": "A.V.",
          "value": 55,
          "phase": "final",
          "verbatim": "55"
        }
      ],
      "remarks": "During feeding  found slight exotherm ,\nVery fine yellow tincture found , slight grip in viscosity found"
    },
    {
      "step": 2,
      "materials": [
        {
          "name": "Step- 1 product",
          "quantity": 152,
          "unit": "g",
          "role": "intermediate"
        },
        {
          "name": "Lupasol G-20 WF",
          "quantity": 13.8,
          "unit": "g",
          "role": "reactant"
        }
      ],
      "procedure": [
        {
          "seq": 1,
          "temperature": "40",
          "time_h": "0.5",
          "atmosphere": "N2",
          "action": "Ramp stage 1"
        },
        {
          "seq": 2,
          "temperature": "65",
          "time_h": "2",
          "atmosphere": "N2",
          "action": "Ramp stage 2"
        }
      ],
      "conditions": {
        "temperature": "40 / 65",
        "atmosphere": "N2",
        "time_h": "0.5 / 2"
      },
      "results": [
        {
          "parameter": "A.V.",
          "value": 48,
          "phase": "final",
          "verbatim": "AV-48"
        },
        {
          "parameter": "amine value",
          "value": 42,
          "phase": "final",
          "verbatim": "Amine value-42"
        }
      ]
    }
  ],
  "observations": "Expt Table remarks: During feeding  found slight exotherm ,\nVery fine yellow tincture found , slight grip in viscosity found"
}