Observations
Expt Table remarks: For Carbon black pigment-Gloss, Tinting strength, Shade good having adhesion dots while cleaning Ink removal Batch 2=3<4<5
Raw materials (collected from the per-step charges)
| Step | Material | Qty | Role |
|---|---|---|---|
| 1 | MPEG-350 | 300 g | reactant |
| 1 | Phosphorous pentaoxide | 9.9 g | reactant |
| 2 | Step 1- Product | 152 g | intermediate |
| 2 | Lupasol G-20 WF | 11 g | reactant |
Process
| Step | Conditions | Charged | What happened | Results |
|---|---|---|---|---|
|
Step 1
28112025 9076 Expt Table 2025.xls
|
temperature: 35 / 55 / 75atmosphere: N2time_h: 0.15 / 0.5 / 1-2 |
MPEG-350 300g Phosphorous pentaoxide 9.9g
|
During feeding of P-RM found slight exotherm Very fine yellow tincture found ,
slight grip in viscosity found, | Initially found brownish dots with exotherm later on changed to pale yellow.
In Final product added -EHA/ Toluene/ Methoxy propyl acetate 3.33% each( by weight %)
—
|
A.V. 41 |
|
Step 2
28112025 9076 Expt Table 2025.xls
|
temperature: 35 / 55 / 60atmosphere: N2time_h: 0.15 / 1 / 2 |
Step 1- Product 152g Lupasol G-20 WF 11g
|
In Final product added -EHA/ Toluene/ Methoxy propyl acetate 3.33% each( by weight %)
—
|
A.V. 40 amine value 45 |
Sample S 9076 #L02060125
result
Violet 23 (NC-PU ink)
| Parameter | This sample | Standard (BYK 9076 Standard) |
|---|---|---|
| Viscosity | 45 sec | 42 sec |
| Gloss | 63.9 | 64.6 |
| Colour Strength | 98 - 99% | 1 |
| Resolubility | 5 | 4 |
| Transparency | Eq. to Std | Ref as Std |
APP DATA- BYK 9076 equivalent.xlsx
result
Violet 27 (NC-PU ink)
| Parameter | This sample | Standard (BYK 9076 Standard) |
|---|---|---|
| Viscosity | 40 sec | 39 sec |
| Gloss | 7.9 | 6.8 |
| Colour Strength | 1 | 1 |
| Resolubility | 2 | 4 |
| Transparency | Slightly redder | Ref as Std |
APP DATA- BYK 9076 equivalent.xlsx
Where this record comes from
APP DATA- BYK 9076 equivalent.xlsx
— application testing · linked by a person
28112025 9076 Expt Table 2025.xls
— researcher summary (cross-check)
Something wrong on this page? Record a correction
Your correction is permanent: it survives every re-extraction and the field can no longer be changed by the system.
Field-by-field provenance (5 fields) — for auditors
2 extraction fragments · merged 2026-08-25 · 0 human-validated fields
Fix a wrong or missing extraction side-by-side with the original:
app-data--S 9076 #L02060125
expt-block--2
| Field | Source | Extractor | Conf. |
|---|---|---|---|
| samples[0] | APP DATA- BYK 9076 equivalent.xlsx sheet BYK_9076_equivalent, rows 82-82 | parse_app_data.py@unversioned | high |
| record_type | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '2', csv rows 6-8 | qwen-tasks/extract-expt-block.md@unversioned | high |
| process_steps[0] | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '2', csv rows 6-8 | qwen-tasks/extract-expt-block.md@unversioned | high |
| process_steps[1] | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '2', csv rows 6-8 | qwen-tasks/extract-expt-block.md@unversioned | high |
| observations | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '2', csv rows 6-8 | qwen-tasks/extract-expt-block.md@unversioned | high |
Raw record JSON
{
"record_id": "exp-9076-002",
"project": "9076",
"aliases": [
"S 9076 #L02060125",
"2",
"Batch 2"
],
"provenance": {
"fragments": [
"app-data--S 9076 #L02060125",
"expt-block--2"
],
"field_provenance": {
"samples[0]": {
"source_file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx",
"extractor": "parse_app_data.py",
"extractor_version": "unversioned",
"extracted_date": "2026-08-19",
"locator": "sheet BYK_9076_equivalent, rows 82-82",
"human_checked": true
},
"record_type": {
"source_file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"extractor": "qwen-tasks/extract-expt-block.md",
"extractor_version": "unversioned",
"extracted_date": "2026-08-19",
"locator": "sheet 9076_Experiments, batch block '2', csv rows 6-8",
"human_checked": true
},
"process_steps[0]": {
"source_file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"extractor": "qwen-tasks/extract-expt-block.md",
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"extracted_date": "2026-08-19",
"locator": "sheet 9076_Experiments, batch block '2', csv rows 6-8",
"human_checked": true
},
"process_steps[1]": {
"source_file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"extractor": "qwen-tasks/extract-expt-block.md",
"extractor_version": "unversioned",
"extracted_date": "2026-08-19",
"locator": "sheet 9076_Experiments, batch block '2', csv rows 6-8",
"human_checked": true
},
"observations": {
"source_file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"extractor": "qwen-tasks/extract-expt-block.md",
"extractor_version": "unversioned",
"extracted_date": "2026-08-19",
"locator": "sheet 9076_Experiments, batch block '2', csv rows 6-8",
"human_checked": true
}
},
"last_merged": "2026-08-25"
},
"documents": [
{
"file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx",
"role": "application_test",
"link_basis": "human link (exp-9076-002)",
"link_status": "user-confirmed"
},
{
"file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"role": "summary_table",
"link_basis": "alias match: 2",
"link_status": "rule"
}
],
"validation": {
"validated_fields": {},
"corrections_applied": []
},
"samples": [
{
"sample_id": "S 9076 #L02060125",
"application_tests": [
{
"test": "Violet 23",
"system": "NC-PU ink",
"conditions": "trial 08.01.2025",
"result": "Viscosity: 45 sec; Gloss: 63.9; Colour Strength: 98 - 99%; Resolubility: 5; Transparency: Eq. to Std",
"vs_reference": "BYK 9076 Standard — Viscosity: 42 sec; Gloss: 64.6; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
"file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
},
{
"test": "Violet 27",
"system": "NC-PU ink",
"conditions": "trial 08.01.2025",
"result": "Viscosity: 40 sec; Gloss: 7.9; Colour Strength: 1; Resolubility: 2; Transparency: Slightly redder",
"vs_reference": "BYK 9076 Standard — Viscosity: 39 sec; Gloss: 6.8; Colour Strength: 1; Resolubility: 4; Transparency: Ref as Std",
"file": "docs/Application data Summary/APP DATA- BYK 9076 equivalent.xlsx"
}
]
}
],
"record_type": "synthesis",
"process_steps": [
{
"step": 1,
"materials": [
{
"name": "MPEG-350",
"quantity": 300,
"unit": "g",
"role": "reactant"
},
{
"name": "Phosphorous pentaoxide",
"quantity": 9.9,
"unit": "g",
"role": "reactant"
}
],
"procedure": [
{
"seq": 1,
"temperature": "35",
"time_h": "0.15",
"atmosphere": "N2",
"action": "Ramp stage 1",
"observation": "During feeding of P-RM found slight exotherm Very fine yellow tincture found , slight grip in viscosity found,"
},
{
"seq": 2,
"temperature": "55",
"time_h": "0.5",
"atmosphere": "N2",
"action": "Ramp stage 2"
},
{
"seq": 3,
"temperature": "75",
"time_h": "1-2",
"atmosphere": "N2",
"action": "Ramp stage 3",
"observation": "Initially found brownish dots with exotherm later on changed to pale yellow."
}
],
"conditions": {
"temperature": "35 / 55 / 75",
"atmosphere": "N2",
"time_h": "0.15 / 0.5 / 1-2"
},
"results": [
{
"parameter": "A.V.",
"value": 41,
"phase": "final",
"verbatim": "41"
}
],
"remarks": "During feeding of P-RM found slight exotherm Very fine yellow tincture found ,\n slight grip in viscosity found, | Initially found brownish dots with exotherm later on changed to pale yellow.\nIn Final product added -EHA/ Toluene/ Methoxy propyl acetate 3.33% each( by weight %)"
},
{
"step": 2,
"materials": [
{
"name": "Step 1- Product",
"quantity": 152,
"unit": "g",
"role": "intermediate"
},
{
"name": "Lupasol G-20 WF",
"quantity": 11,
"unit": "g",
"role": "reactant"
}
],
"procedure": [
{
"seq": 1,
"temperature": "35",
"time_h": "0.15",
"atmosphere": "N2",
"action": "Ramp stage 1"
},
{
"seq": 2,
"temperature": "55",
"time_h": "1",
"atmosphere": "N2",
"action": "Ramp stage 2"
},
{
"seq": 3,
"temperature": "60",
"time_h": "2",
"atmosphere": "N2",
"action": "Ramp stage 3"
}
],
"conditions": {
"temperature": "35 / 55 / 60",
"atmosphere": "N2",
"time_h": "0.15 / 1 / 2"
},
"results": [
{
"parameter": "A.V.",
"value": 40,
"phase": "final",
"verbatim": "AV- 40, \nAmine value- 45"
},
{
"parameter": "amine value",
"value": 45,
"phase": "final",
"verbatim": "AV- 40, \nAmine value- 45"
}
],
"remarks": "In Final product added -EHA/ Toluene/ Methoxy propyl acetate 3.33% each( by weight %)"
}
],
"observations": "Expt Table remarks: For Carbon black pigment-Gloss, Tinting strength, Shade good \nhaving adhesion dots while cleaning Ink removal Batch 2=3<4<5"
}