Nothing extracted for this section yet.
Raw materials (collected from the per-step charges)
| Step | Material | Role |
|---|---|---|
| 1 | Butanol EO/PO BEP-55 (110 gm HV-88) Unitop RM | - |
| 1 | Phosphorous pentaoxide | - |
| 2 | Step-1 Product | intermediate |
| 2 | Lupasol G-20 WF | - |
Process
| Step | Conditions | Charged | What happened | Results |
|---|---|---|---|---|
|
Step 1
28112025 9076 Expt Table 2025.xls
|
temperature: 60 / 65atmosphere: N2time_h: 1 / 4 |
Butanol EO/PO BEP-55 (110 gm HV-88) Unitop RM Phosphorous pentaoxide
|
— | |
|
Step 2
28112025 9076 Expt Table 2025.xls
|
temperature: 58 / 61atmosphere: N2time_h: 1 / 3 |
Step-1 Product Lupasol G-20 WF
|
— | acid_value 37 amine_value 29 |
No test results linked to this batch yet.
Where this record comes from
28112025 9076 Expt Table 2025.xls
— researcher summary (cross-check)
Something wrong on this page? Record a correction
Your correction is permanent: it survives every re-extraction and the field can no longer be changed by the system.
Field-by-field provenance (2 fields) — for auditors
1 extraction fragments · merged 2026-08-25 · 0 human-validated fields
Fix a wrong or missing extraction side-by-side with the original:
expt-block--18
| Field | Source | Extractor | Conf. |
|---|---|---|---|
| process_steps[0] | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '18', csv rows 60-61 | qwen-tasks/extract-expt-block.md@unversioned | high |
| process_steps[1] | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '18', csv rows 60-61 | qwen-tasks/extract-expt-block.md@unversioned | high |
Raw record JSON
{
"record_id": "exp-9076-018",
"project": "9076",
"aliases": [
"18"
],
"provenance": {
"fragments": [
"expt-block--18"
],
"field_provenance": {
"process_steps[0]": {
"source_file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"extractor": "qwen-tasks/extract-expt-block.md",
"extractor_version": "unversioned",
"extracted_date": "2026-08-20",
"locator": "sheet 9076_Experiments, batch block '18', csv rows 60-61",
"human_checked": true
},
"process_steps[1]": {
"source_file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"extractor": "qwen-tasks/extract-expt-block.md",
"extractor_version": "unversioned",
"extracted_date": "2026-08-20",
"locator": "sheet 9076_Experiments, batch block '18', csv rows 60-61",
"human_checked": true
}
},
"last_merged": "2026-08-25"
},
"documents": [
{
"file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"role": "summary_table",
"link_basis": "alias match: 18",
"link_status": "rule"
}
],
"validation": {
"validated_fields": {},
"corrections_applied": []
},
"process_steps": [
{
"step": 1,
"materials": [
{
"name": "Butanol EO/PO BEP-55 (110 gm HV-88) Unitop RM",
"qty_g": "110",
"role": "unknown",
"role_verbatim": "raw_material"
},
{
"name": "Phosphorous pentaoxide",
"qty_g": "2.53",
"role": "unknown",
"role_verbatim": "raw_material"
}
],
"procedure": [
{
"seq": 1,
"temperature": "60",
"time_h": "1",
"verbatim": "60 / 1 hrs"
},
{
"seq": 2,
"temperature": "65",
"time_h": "4",
"atmosphere": "N2",
"verbatim": "65 / 4 hrs / N2"
}
],
"conditions": {
"temperature": "60 / 65",
"atmosphere": "N2",
"time_h": "1 / 4"
},
"results": [
{
"parameter": "unlabelled",
"value": "47",
"verbatim": "A.V. cell: 47"
}
],
"remarks": ""
},
{
"step": 2,
"materials": [
{
"name": "Step-1 Product",
"qty_g": "110",
"role": "intermediate"
},
{
"name": "Lupasol G-20 WF",
"qty_g": "5.2",
"role": "unknown",
"role_verbatim": "raw_material"
}
],
"procedure": [
{
"seq": 1,
"temperature": "58",
"time_h": "1",
"verbatim": "58 / 1 hr"
},
{
"seq": 2,
"temperature": "61",
"time_h": "3",
"atmosphere": "N2",
"verbatim": "61 / 3 hr / N2"
}
],
"conditions": {
"temperature": "58 / 61",
"atmosphere": "N2",
"time_h": "1 / 3"
},
"results": [
{
"parameter": "acid_value",
"value": "37",
"verbatim": "AV-37"
},
{
"parameter": "amine_value",
"value": "29",
"verbatim": "Amine value-29/"
}
],
"remarks": ""
}
]
}