Observations
Expt Table remarks: AV-41.5/ SAP- 80
Raw materials (collected from the per-step charges)
| Step | Material | Role |
|---|---|---|
| 1 | Vicasurf 1010 (HV-115-120) | - |
| 1 | Polyphosphoric acid | - |
| 2 | Epomine SP- 018 | - |
| 2 | 2 ethyl hexyl acrylate | - |
| 3 | Step- 1 product (78) | intermediate |
| 3 | Step - 2 Product (20) | intermediate |
Process
| Step | Conditions | Charged | What happened | Results |
|---|---|---|---|---|
|
Step 1
28112025 9076 Expt Table 2025.xls
|
temperature: 65 / 75atmosphere: N2time_h: 2 / 3.5 |
Vicasurf 1010 (HV-115-120) Polyphosphoric acid
|
— | acid_value 44 acid_value 48 SAP 81 HV 120 |
|
Step 2
28112025 9076 Expt Table 2025.xls
|
temperature: 75 / 80atmosphere: N2time_h: 2 / 4.5 |
Epomine SP- 018 2 ethyl hexyl acrylate
|
— | amine_value 263 SAP 197 HV 170 IV 42 |
|
Step 3
28112025 9076 Expt Table 2025.xls
|
temperature: 60 / 65atmosphere: N2time_h: 2 / 5 |
Step- 1 product (78) Step - 2 Product (20)
|
— | acid_value 41.5 SAP 80 IV 12 HV 136.5 amine_value 42.195 |
No test results linked to this batch yet.
Where this record comes from
28112025 9076 Expt Table 2025.xls
— researcher summary (cross-check)
Something wrong on this page? Record a correction
Your correction is permanent: it survives every re-extraction and the field can no longer be changed by the system.
Field-by-field provenance (4 fields) — for auditors
1 extraction fragments · merged 2026-08-25 · 0 human-validated fields
Fix a wrong or missing extraction side-by-side with the original:
expt-block--17
| Field | Source | Extractor | Conf. |
|---|---|---|---|
| process_steps[0] | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '17', csv rows 57-58 | qwen-tasks/extract-expt-block.md@unversioned | high |
| process_steps[1] | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '17', csv rows 57-58 | qwen-tasks/extract-expt-block.md@unversioned | high |
| process_steps[2] | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '17', csv rows 57-58 | qwen-tasks/extract-expt-block.md@unversioned | high |
| observations | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '17', csv rows 57-58 | qwen-tasks/extract-expt-block.md@unversioned | high |
Raw record JSON
{
"record_id": "exp-9076-017",
"project": "9076",
"aliases": [
"17"
],
"provenance": {
"fragments": [
"expt-block--17"
],
"field_provenance": {
"process_steps[0]": {
"source_file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"extractor": "qwen-tasks/extract-expt-block.md",
"extractor_version": "unversioned",
"extracted_date": "2026-08-20",
"locator": "sheet 9076_Experiments, batch block '17', csv rows 57-58",
"human_checked": true
},
"process_steps[1]": {
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"extractor_version": "unversioned",
"extracted_date": "2026-08-20",
"locator": "sheet 9076_Experiments, batch block '17', csv rows 57-58",
"human_checked": true
},
"process_steps[2]": {
"source_file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"extractor": "qwen-tasks/extract-expt-block.md",
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"extracted_date": "2026-08-20",
"locator": "sheet 9076_Experiments, batch block '17', csv rows 57-58",
"human_checked": true
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"observations": {
"source_file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"extractor": "qwen-tasks/extract-expt-block.md",
"extractor_version": "unversioned",
"extracted_date": "2026-08-20",
"locator": "sheet 9076_Experiments, batch block '17', csv rows 57-58",
"human_checked": true
}
},
"last_merged": "2026-08-25"
},
"documents": [
{
"file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"role": "summary_table",
"link_basis": "alias match: 17",
"link_status": "rule"
}
],
"validation": {
"validated_fields": {},
"corrections_applied": []
},
"process_steps": [
{
"step": 1,
"materials": [
{
"name": "Vicasurf 1010 (HV-115-120)",
"qty_g": "450",
"role": "unknown",
"role_verbatim": "raw_material"
},
{
"name": "Polyphosphoric acid",
"qty_g": "16.18",
"role": "unknown",
"role_verbatim": "raw_material"
}
],
"procedure": [
{
"seq": 1,
"temperature": "65",
"time_h": "2",
"atmosphere": "N2",
"verbatim": "65 / 2 / N2"
},
{
"seq": 2,
"temperature": "75",
"time_h": "3.5",
"verbatim": "75 / 3.5"
}
],
"conditions": {
"temperature": "65 / 75",
"atmosphere": "N2",
"time_h": "2 / 3.5"
},
"results": [
{
"parameter": "acid_value",
"value": "44",
"verbatim": "A.V. cell: AV-44"
},
{
"parameter": "acid_value",
"value": "48",
"verbatim": "A.V. cell: Final AV-48 \\nSAP-81/ HV-120"
},
{
"parameter": "SAP",
"value": "81",
"verbatim": "A.V. cell: Final AV-48 \\nSAP-81/ HV-120"
},
{
"parameter": "HV",
"value": "120",
"verbatim": "A.V. cell: Final AV-48 \\nSAP-81/ HV-120"
}
],
"remarks": ""
},
{
"step": 2,
"materials": [
{
"name": "Epomine SP- 018",
"qty_g": "60",
"role": "unknown",
"role_verbatim": "raw_material"
},
{
"name": "2 ethyl hexyl acrylate",
"qty_g": "140",
"role": "unknown",
"role_verbatim": "raw_material"
}
],
"procedure": [
{
"seq": 1,
"temperature": "75",
"time_h": "2",
"verbatim": "75 / 2"
},
{
"seq": 2,
"temperature": "80",
"time_h": "4.5",
"atmosphere": "N2",
"verbatim": "80 / 4.5 / N2"
}
],
"conditions": {
"temperature": "75 / 80",
"atmosphere": "N2",
"time_h": "2 / 4.5"
},
"results": [
{
"parameter": "amine_value",
"value": "263",
"verbatim": "A.V. cell: amine - 263/"
},
{
"parameter": "SAP",
"value": "197",
"verbatim": "A.V. cell: SAP- 197/\\n HV-170/IV-42"
},
{
"parameter": "HV",
"value": "170",
"verbatim": "A.V. cell: SAP- 197/\\n HV-170/IV-42"
},
{
"parameter": "IV",
"value": "42",
"verbatim": "A.V. cell: SAP- 197/\\n HV-170/IV-42"
}
],
"remarks": ""
},
{
"step": 3,
"materials": [
{
"name": "Step- 1 product (78)",
"qty_g": "78",
"role": "intermediate"
},
{
"name": "Step - 2 Product (20)",
"qty_g": "20",
"role": "intermediate"
}
],
"procedure": [
{
"seq": 1,
"temperature": "60",
"time_h": "2",
"verbatim": "60 / 2"
},
{
"seq": 2,
"temperature": "65",
"time_h": "5",
"atmosphere": "N2",
"verbatim": "65 / 5 / N2"
}
],
"conditions": {
"temperature": "60 / 65",
"atmosphere": "N2",
"time_h": "2 / 5"
},
"results": [
{
"parameter": "acid_value",
"value": "41.5",
"verbatim": "Remarks cell: AV-41.5/ SAP- 80"
},
{
"parameter": "SAP",
"value": "80",
"verbatim": "Remarks cell: AV-41.5/ SAP- 80"
},
{
"parameter": "IV",
"value": "12",
"verbatim": "A.V. cell: IV-12/HV-136.5/ \\nAmine value-42.195"
},
{
"parameter": "HV",
"value": "136.5",
"verbatim": "A.V. cell: IV-12/HV-136.5/ \\nAmine value-42.195"
},
{
"parameter": "amine_value",
"value": "42.195",
"verbatim": "A.V. cell: IV-12/HV-136.5/ \\nAmine value-42.195"
}
],
"remarks": ""
}
],
"observations": "Expt Table remarks: AV-41.5/ SAP- 80"
}