Pipeline
Turn the document drop into verified experiment records — work the steps left to right.
1
Discoversee what's in the drop
2
Extractdocuments → data, checked as you go
3
Linkconnect to experiments
4
Browsethe experiment records
← 28112025 9076 Expt Table 2025.xls · fragment 55 of 66 from this file
Original · 28112025 9076 Expt Table 2025.xls
open ↗Sheet · 28112025 9076 Expt Table 2025.converted_sheet_9076_Experiments.csv — rows 324–401 of 400 · cited row highlighted
| (P-1.2 %) | 76-78 | 0.5 hr feed ove\nr slight yellow\n tincture, clear\n transparent mass | 30 min | 55 | Feed of Phosphate (50%) | clear mass | |||||||||||||
| AV-39.65/ SAP-40.48 | 78-79 | 1 hr clear transparent with slight yellow tincture\n // Feed over | 20 min | 55 | 0.3 | yellow brownish clear | |||||||||||||
| 10 min | 56 | 20 % feed completed | viscosity incresed | ||||||||||||||||
| 78-81 | 2 hr clear\n transparent\n yellow tincture \nreaction mass. | AV-0.3/ Amine-290.5/\n IV-30/HV-218.14 | 1.5 hr | 57-58 | stirrer well | ||||||||||||||
| 78-81 | 2 hr clear transparent increase\n yellow tincture \nreaction mass. | 3 hr IV-45\n6.5 IV 30\n | Cool | AV-33.2/SAP-59.4/Amine- \n/ HV-70.5/IV-8.7 | |||||||||||||||
| 38C | i) Surfol R-1400 HV-36.8 (R-83/) | 226 | 54 | 0.5 | i) Lupasol G-20 WF | Step - 1 Product( | 160(80%) | AV-43.1 | |||||||||||
| ii) PolyPhosphoric acid (102%) | 4.023 | 56 | 1 | ii) 2 ethyl hexyl acrylate | Same as in\n LBN-38 D | Step - 2 Product( L-2) | 40 (20%) | ||||||||||||
| ii) Phosphorous pentaoxide | 3.14 | 68 | 1.5 | AV-43.1 | 10 | 55 | Stirre well | N-2 | yellowish | ||||||||||
| (P-1.2 %) | 15min | 55 | Feed of Phosphate (50%) | clear mass | |||||||||||||||
| 20 min | 55 | feed completed | yellow brownish clear | ||||||||||||||||
| PPA feed at 55 deg C for 10 min | 55 deg | 72-76 deg | 45 min | viscosity incresed | |||||||||||||||
| P2O5 feed at 55 deg C for 10 min | 55 | 76-78 | 1.5 hr | AV-0.3/ Amine-290.5/\n IV-30/HV-218.14 | 1.5 hr | 57-58 | stirrer well | AV-36.9/ SAP-50.6/HV71.89/ IV-7.377\nAmine-47.5 | |||||||||||
| Cool | |||||||||||||||||||
| 39 | i) Surfol R-1400 / MW 1500 ( 2 kg) \nR-188 | 265 | 54 | 0.5 | i) Epomine SP- 018 | 90 | Step - 1 Product | 240 | AV-35.5 | ||||||||||
| ii) PolyPhosphoric acid (106%) | 4.67 | 56 | 2.5 | ii) 2 ethyl hexyl acrylate | 210 | Step - 2 Product | 60 | ||||||||||||
| ii) Phosphorous pentaoxide | 3.65 | 68 | 2 | iii) AIBN | 0.6 gm | 55 | Stirre well | N-2 | |||||||||||
| 30 min | 55 | Feed of Phosphate | N-2 | ||||||||||||||||
| PPA feed at 55 deg C for 10 min | 55 | 0.1 | RBF with SP-18 | 79 | 10 min | 55 | Turbidity found | N-2 | |||||||||||
| 77 | 2.5 | AIBN 0.6 gm added | 79 deg C | 10 min stirrerd | 30 min | 55 | Turbidity reduced | N-2 | |||||||||||
| Started feed 2 EH acrylate | 79-81 | 2 hr | 30 min | 58 | Turbidity reduced | N-2 | |||||||||||||
| P2O5 feed at 55 deg C for 10 min | 55 | 0.1 | 78-82 | 3.5 | IV- 42 | 30 | 57-59 | Found foam in\n reaction mass | N-2 | ||||||||||
| 75-78 | 2.5 | AV-35.6/\n SAP39.5/\nHV-37.6 | 78-82 | 5.5 | IV- 27.5 | AV-1.5/SAP-204/\nHV-183/Amine-285/IV-27.5 | 1.5 hr | 57-59 | Found foam at\n top of mass | AV-29.67/SAP-71.87/\nHV-44.67/Amine-46.5/\nIV-9.4 | |||||||||
| After ward heated on heating mantle | 82-85 | 1.5 hr | Cool to RT | ||||||||||||||||
| i) Epomine SP- 018 | 90 | Step - 1 Product | 80 gm | ||||||||||||||||
| 40 | R-1400 R-188 (1000) | 157 | 40 | 0.2 | ii) 2 ethyl hexyl acrylate | 210 | Step - 2 Product | 20 gm | 55-60 | feeding of Step-I over 25-30 min | |||||||||
| PPA ( 106 %) | 5.74 | 70-75 | 3.5 | AV-44.3 | iii) AIBN | 0.6 gm | |||||||||||||
| RBF with SP-18 | 79 | ||||||||||||||||||
| AIBN 0.6 gm added | 79 deg C | 10 min stirrerd | |||||||||||||||||
| Started feed 2 EH acrylate | 79-81 | 2 hr | |||||||||||||||||
| 78-82 | 3.5 | IV- 42 | |||||||||||||||||
| 78-82 | 5.5 | IV- 27.5 | AV-1.5/SAP-204/\nHV-183/Amine-285/IV-27.5 | ||||||||||||||||
| 41 | i) Esteem BEP 1450 ( HV-40 LOD-3.1 %) / Lot-2505013A/ R-2433 | 350 gm | 45 | 0.2 | Epomine SP- 018 | 225 | 74-81 | 2 | Feed | Step - 1 Product\nPhosphate | 0.8 | ||||||||
| 05.06.25 | ii) Phosphorous pentaoxide | 13 gm | 70-75 | 1 | Found coagulant later on dispersed | 2 ethyl hexyl acrylate | 525 | 78-82 | 6 | N2 | AV- \n / Amine -\nIV-27.5 | Step - 2 Product\nAcrylate | 0.2 | 55-60 | 0.2 hr / dispersed well | AV-36.8/SAP-52.5/Amine-38.7/HV-76.2/IV-7.9 | |||
| 74-75 | 2.5 | yellowish liq. Traces of particles | Iodine value | Time | 55-60 | 0.5 hr feed of phosphate ester | |||||||||||||
| 67 | 3.5 | 55-60 | 2.5 hr stirred well | ||||||||||||||||
| 28 | 5.5 | Tested for Violet-23 & Black | |||||||||||||||||
| Both pigment resolubility fail | |||||||||||||||||||
| 42 | i) Esteem BEP 1450 ( HV-40 LOD-3.1 %) Lot-2505013A\nR-2433 | 200 gm | 40 | 0.2 | Epomine SP- 018 | 72.8 | 74-81 | 2 | Feed | Step - 1 Product\nPhosphate | 0.85 | ||||||||
| 26.6.25 | ii) Phosphorous pentaoxide | 5.9 gm | 70-75 | 1 | Brownish crystal | 2 ethyl hexyl acrylate | 169.1 | 78-82 | 6 | N2 | AV- \n / Amine -\nIV-27.5 | Step - 2 Product\nAcrylate | 0.15 | 55-60 | 0.2 hr / dispersed well | AV-32.6/ SAP-64/Amine-40.5/IV-6.2 | |||
| 74-75 | 3 | AV-36.85 | Iodine value | Time | 55-60 | 0.5 hr feed of phosphate ester | |||||||||||||
| 55 | 3 | 55-60 | 2.5 hr stirred well turbidity found | ||||||||||||||||
| 27.5 | 5.5 | Non uniform mass | |||||||||||||||||
| Mono-15.5/ Di-72/Free A-0.53 | |||||||||||||||||||
| 48 | i) Vicaspin LUB 1010 (R225100845) Bu- EO-PO\nHV-62.3/ MW-900 | 178 | 45 | 0.2 | i) Epomine SP- 018 | 30 | 0.2 | 80 | Step - 1 Product\nPhosphate ester | 0.85 | P-1.82% | ||||||||
| 20.10.25 | ii) Phosphorous pentaoxide | 9.357 | 75 | 3.5 | Clear mass no particlesAV-52.52 | ii) 2 ethyl hexyl acrylate | 70 | 2 | 79-81 | Feed of RM-II | Step - 2 Product \nAcrylate | 0.15 | 0.5 | Heating acrylate intermediate \n@ 55 deg C | |||||
| P-2.14% | Mono-24.44 / Di- 51.76/ Free acid-0.24 | 0.5 | Feed of phosphate ester | ||||||||||||||||
| 5.5 | 79-81 | IV-26.1 @ 5.5 hrs | 3.5 | Stirrer well , clear \ntransparent mass | AV-44.36/ HV-46.58/SAP-62.14\n/Amine-36.25/ IV-5.8 | ||||||||||||||
| Yellowish clear \ntransparent mass | Tested over pigment Black, Blue, Violet-23/27 etc\nAll having matching resolubility while reduced gloss in violet | ||||||||||||||||||
| RM from above Batch | |||||||||||||||||||
| LBN-48 (Q) | i) Acrylate | 0.15 | |||||||||||||||||
| ii) Dimethyl sulphate | 0.005 | 65-75 | 1 hr | Clear transparent mass | |||||||||||||||
| iii) Phosphate | 0.85 | 55-60 | 2.5 hr | Yellowish transparent \nclear mass | |||||||||||||||
| AV-52/Amine-31.67\n/IV-3.48/SAP-84.9/HV-38.6 | Tested on Violet 23\n resolubility ok | ||||||||||||||||||
| 49 | i) Vicaspin LUB 1010 (R225100845) Bu- EO-PO\nHV-62.3/ MW-900 | 208 | 45 | 0.2 | i) Epomine SP- 018 | 30 | 0.2 | 80 | Step - 1 Product\nPhosphate ester | 0.87 | P-1.86 % | AV-46.5/ HV-49.4/SAP-61.98\n/Amine-20.2/ IV-2.58 | |||||||
| 1.11.2025 | ii) Phosphorous pentaoxide | 10.93 | 75 | 3.5 | Clear mass no particles AV-51.87 | ii) 2 ethyl hexyl acrylate | 70 | 2 | 79-81 | Feed of RM-II | Step - 2 Product \nAcrylate | 0.13 | 0.5 | Heating acrylate intermediate \n@ 55 deg C | Tested over pigment Black, Blue, Violet-23/27 etc\nAll having matching resolubility in black, blue & viloet 27 while slight reduced in gloss found in all pigments | ||||
| P-2.14% | Mono-22.56 / Di- 48.93/ Free acid-1.096 | 0.5 | Feed of phosphate ester | ||||||||||||||||
| 5.5 | 79-81 | IV-26.1 @ 5.5 hrs | 3.5 | Stirrer well , clear \ntransparent mass | |||||||||||||||
| 50 | i) Vicaspin LUB 1010 (R225100845) Bu- EO-PO\nHV-62.3/ MW-900 | 301 | 45 | 0.2 | Clear mass no particles | i) Epomine SP- 018 | 30 | 0.2 | 80 | B.No- 50B\nStep - 1 Product\nPhosphate ester | 0.8 | P-1.71 % | AV-44.14/Amine-47.1/ IV-4.9/ \nSAP-84.29/HV-58.5 | ||||||
| 5.11.25 | ii) Phosphorous pentaoxide | 15.82 | 75 | 3.5 | AV-52.5 | ii) 2 ethyl hexyl acrylate | 70 | 2 | 79-81 | Feed of RM-II | Step - 2 Product \nAcrylate | 0.2 | 0.5 | Heating acrylate intermediate \n@ 55 deg C | Tested on Black & violet pigment \nResolubility less while other parameters nearby | ||||
| Mono-23.5 / Di- 53.2/ Free acid-0.1 | 0.5 | Feed of phosphate ester | |||||||||||||||||
| P-2.14% | 5.5 | 79-81 | IV-26.1 @ 5.5 hrs | 3.5 | Stirrer well , clear \ntransparent mass | ||||||||||||||
| Yellowish clear \ntransparent mass | |||||||||||||||||||
| B.No-50 A | i) Acrylate (15%) 37.5 | 65-70 | 0.2 | ||||||||||||||||
| ii) DMS (1%) 2.52 | Feed over 15 min | ||||||||||||||||||
| 70-75 | 1.5 hr clear yellowish\n mass | ||||||||||||||||||
| iii) Phosphate ester- (85%) 212.5 | 55-62 | 0.5 hr feed of RM-III) | |||||||||||||||||
| 58-62 | 3 hr/ Clear uniform mass\nSlight turbidity | ||||||||||||||||||
| AV-48.7/amine-31.08 /IV-4.58\n/SAP-88.4/HV-45.5 | Tested on Black & violet pigment \nResolubility less while other parameters nearby |
Extracted values
… checked
Cited: sheet 9076_Experiments, batch block '40', csv rows 354-361 (highlighted). Compare with the original on the left.
Press Enter to OK the highlighted value, or click OK / fix on any value.
Experiment: exp-9076-040
✓ Every value checked — fragment marked reviewed.
All checked — go to Link →
Process steps
| Step | Charged | What happened | Results | ||||||||||||||||||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
|
Step 1
temperature 40; 70-75 time_h 0.2 h; 3.5 h
|
R-1400 R-188 · 157
PPA · 5.74
|
|
— | ||||||||||||||||||||||||||||||
|
Step 2
temperature 78-82 time_h 3.5 h; 5.5 h
|
2 ethyl hexyl acrylate · 210
AIBN · 0.6 gm
|
|
iodine_value 42
iodine_value 27.5
acid_value 44.3
|
||||||||||||||||||||||||||||||
|
Step 3
temperature 55-60 time_h 25-30 min (feed of Step-I)
|
Step - 2 Product · 20 gm
|
|
acid_value 1.5
saponification_value 204
hv 183
amine_value 285
iodine_value 27.5
|
[
{
"conditions": {
"temperature": "40; 70-75",
"time_h": "0.2 h; 3.5 h"
},
"materials": [
{
"name": "R-1400 R-188",
"qty_g": "157",
"role": "reactant",
"verbatim": "R-1400 R-188 (1000)"
},
{
"name": "PPA",
"qty_g": "5.74",
"role": "reactant",
"verbatim": "PPA ( 106 %)"
}
],
"procedure": [
{
"seq": 1,
"temperature": "40",
"time_h": "0.2",
"type": "temperature",
"verbatim": "40 / 0.2"
},
{
"seq": 2,
"temperature": "70-75",
"time_h": "3.5",
"type": "temperature",
"verbatim": "70-75 / 3.5"
},
{
"seq": 3,
"type": "condition",
"verbatim": "RBF with SP-18"
},
{
"event": "AIBN 0.6 gm added",
"seq": 4,
"temperature": "79 deg C",
"time_h": "10 min",
"type": "addition",
"verbatim": "AIBN 0.6 gm added ,79 deg C,10 min stirrerd"
},
{
"event": "Started feed 2 EH acrylate",
"seq": 5,
"temperature": "79-81",
"time_h": "2 hr",
"type": "feed",
"verbatim": "Started feed 2 EH acrylate,79-81,2 hr"
}
],
"remarks": "{\u0027type\u0027: \u0027note\u0027, \u0027text\u0027: \"Step 1 \u0027Other\u0027 column holds prose, not results: \u0027RBF with SP-18\u0027, \u0027AIBN 0.6 gm added\u0027, \u0027Started feed 2 EH acrylate\u0027. Carried as procedure events, not dropped.\"}; {\u0027type\u0027: \u0027note\u0027, \u0027text\u0027: \"Material 1 name cell reads \u0027R-1400 R-188 (1000)\u0027; the \u0027(1000)\u0027 suffix is part of the name cell, not a separate quantity.\"}",
"results": [],
"step": 1
},
{
"conditions": {
"temperature": "78-82",
"time_h": "3.5 h; 5.5 h"
},
"materials": [
{
"name": "2 ethyl hexyl acrylate",
"qty_g": "210",
"role": "reactant",
"verbatim": "ii) 2 ethyl hexyl acrylate"
},
{
"name": "AIBN",
"qty_g": "0.6 gm",
"role": "reactant",
"verbatim": "iii) AIBN"
}
],
"procedure": [
{
"seq": 1,
"temperature": "78-82",
"time_h": "3.5",
"type": "temperature",
"verbatim": "78-82 / 3.5"
},
{
"seq": 2,
"temperature": "78-82",
"time_h": "5.5",
"type": "temperature",
"verbatim": "78-82 / 5.5"
}
],
"remarks": "",
"results": [
{
"parameter": "iodine_value",
"value": "42",
"verbatim": "IV- 42"
},
{
"parameter": "iodine_value",
"value": "27.5",
"verbatim": "IV- 27.5"
},
{
"note": "polysemous \u0027A.V.\u0027 cell of Step 2 (also carries Step 1 acid value by elimination)",
"parameter": "acid_value",
"value": "44.3",
"verbatim": "AV-44.3"
}
],
"step": 2
},
{
"conditions": {
"temperature": "55-60",
"time_h": "25-30 min (feed of Step-I)"
},
"materials": [
{
"name": "Step - 2 Product",
"qty_g": "20 gm",
"role": "intermediate",
"verbatim": "Step - 2 Product"
}
],
"procedure": [
{
"event": "feeding of Step-I over 25-30 min",
"seq": 1,
"temperature": "55-60",
"type": "temperature",
"verbatim": "55-60,feeding of Step-I over 25-30 min"
}
],
"remarks": "{\u0027type\u0027: \u0027note\u0027, \u0027text\u0027: \"Step 3 material reads \u0027Step - 2 Product\u0027 with Qty \u002720 gm\u0027 and a feed event \u0027feeding of Step-I over 25-30 min\u0027. The named material (Step-2 product) and the feed source (Step-I) do not agree; copied verbatim as printed.\"}; {\u0027type\u0027: \u0027note\u0027, \u0027text\u0027: \u0027Step 3 A.V. column is a multi-value result string (AV/SAP/HV/Amine/IV); all values emitted as measurements.\u0027}",
"results": [
{
"parameter": "acid_value",
"value": "1.5",
"verbatim": "AV-1.5/SAP-204/\nHV-183/Amine-285/IV-27.5"
},
{
"parameter": "saponification_value",
"value": "204",
"verbatim": "AV-1.5/SAP-204/\nHV-183/Amine-285/IV-27.5"
},
{
"parameter": "hv",
"value": "183",
"verbatim": "AV-1.5/SAP-204/\nHV-183/Amine-285/IV-27.5"
},
{
"parameter": "amine_value",
"value": "285",
"verbatim": "AV-1.5/SAP-204/\nHV-183/Amine-285/IV-27.5"
},
{
"parameter": "iodine_value",
"value": "27.5",
"verbatim": "AV-1.5/SAP-204/\nHV-183/Amine-285/IV-27.5"
}
],
"step": 3
}
]
More actions — correct a value · link · ignore
History (1)
| Action | Field | Value | Date |
|---|---|---|---|
| verify | 2026-08-20 |
Raw fragment JSON
{
"fragment_id": "expt-block--40",
"source_file": "docs/Project Expt Report/28112025 9076 Expt Table 2025.xls",
"derived_from": "ocr/28112025 9076 Expt Table 2025.converted/28112025 9076 Expt Table 2025.converted_sheet_9076_Experiments.csv",
"locator": "sheet 9076_Experiments, batch block '40', csv rows 354-361",
"extractor": "qwen-tasks/extract-expt-block.md",
"target_aliases": [
"40"
],
"document_role": "summary_table",
"payload": {
"record_type": "synthesis",
"process_steps": [
{
"step": 1,
"materials": [
{
"name": "R-1400 R-188",
"qty_g": "157",
"role": "reactant",
"verbatim": "R-1400 R-188 (1000)"
},
{
"name": "PPA",
"qty_g": "5.74",
"role": "reactant",
"verbatim": "PPA ( 106 %)"
}
],
"procedure": [
{
"seq": 1,
"type": "temperature",
"temperature": "40",
"time_h": "0.2",
"verbatim": "40 / 0.2"
},
{
"seq": 2,
"type": "temperature",
"temperature": "70-75",
"time_h": "3.5",
"verbatim": "70-75 / 3.5"
},
{
"seq": 3,
"type": "condition",
"verbatim": "RBF with SP-18"
},
{
"seq": 4,
"type": "addition",
"temperature": "79 deg C",
"time_h": "10 min",
"event": "AIBN 0.6 gm added",
"verbatim": "AIBN 0.6 gm added ,79 deg C,10 min stirrerd"
},
{
"seq": 5,
"type": "feed",
"temperature": "79-81",
"time_h": "2 hr",
"event": "Started feed 2 EH acrylate",
"verbatim": "Started feed 2 EH acrylate,79-81,2 hr"
}
],
"conditions": {
"temperature": "40; 70-75",
"time_h": "0.2 h; 3.5 h"
},
"results": [],
"remarks": "{'type': 'note', 'text': \"Step 1 'Other' column holds prose, not results: 'RBF with SP-18', 'AIBN 0.6 gm added', 'Started feed 2 EH acrylate'. Carried as procedure events, not dropped.\"}; {'type': 'note', 'text': \"Material 1 name cell reads 'R-1400 R-188 (1000)'; the '(1000)' suffix is part of the name cell, not a separate quantity.\"}"
},
{
"step": 2,
"materials": [
{
"name": "2 ethyl hexyl acrylate",
"qty_g": "210",
"role": "reactant",
"verbatim": "ii) 2 ethyl hexyl acrylate"
},
{
"name": "AIBN",
"qty_g": "0.6 gm",
"role": "reactant",
"verbatim": "iii) AIBN"
}
],
"procedure": [
{
"seq": 1,
"type": "temperature",
"temperature": "78-82",
"time_h": "3.5",
"verbatim": "78-82 / 3.5"
},
{
"seq": 2,
"type": "temperature",
"temperature": "78-82",
"time_h": "5.5",
"verbatim": "78-82 / 5.5"
}
],
"conditions": {
"temperature": "78-82",
"time_h": "3.5 h; 5.5 h"
},
"results": [
{
"parameter": "iodine_value",
"value": "42",
"verbatim": "IV- 42"
},
{
"parameter": "iodine_value",
"value": "27.5",
"verbatim": "IV- 27.5"
},
{
"parameter": "acid_value",
"value": "44.3",
"note": "polysemous 'A.V.' cell of Step 2 (also carries Step 1 acid value by elimination)",
"verbatim": "AV-44.3"
}
],
"remarks": ""
},
{
"step": 3,
"materials": [
{
"name": "Step - 2 Product",
"qty_g": "20 gm",
"role": "intermediate",
"verbatim": "Step - 2 Product"
}
],
"procedure": [
{
"seq": 1,
"type": "temperature",
"temperature": "55-60",
"event": "feeding of Step-I over 25-30 min",
"verbatim": "55-60,feeding of Step-I over 25-30 min"
}
],
"conditions": {
"temperature": "55-60",
"time_h": "25-30 min (feed of Step-I)"
},
"results": [
{
"parameter": "acid_value",
"value": "1.5",
"verbatim": "AV-1.5/SAP-204/\nHV-183/Amine-285/IV-27.5"
},
{
"parameter": "saponification_value",
"value": "204",
"verbatim": "AV-1.5/SAP-204/\nHV-183/Amine-285/IV-27.5"
},
{
"parameter": "hv",
"value": "183",
"verbatim": "AV-1.5/SAP-204/\nHV-183/Amine-285/IV-27.5"
},
{
"parameter": "amine_value",
"value": "285",
"verbatim": "AV-1.5/SAP-204/\nHV-183/Amine-285/IV-27.5"
},
{
"parameter": "iodine_value",
"value": "27.5",
"verbatim": "AV-1.5/SAP-204/\nHV-183/Amine-285/IV-27.5"
}
],
"remarks": "{'type': 'note', 'text': \"Step 3 material reads 'Step - 2 Product' with Qty '20 gm' and a feed event 'feeding of Step-I over 25-30 min'. The named material (Step-2 product) and the feed source (Step-I) do not agree; copied verbatim as printed.\"}; {'type': 'note', 'text': 'Step 3 A.V. column is a multi-value result string (AV/SAP/HV/Amine/IV); all values emitted as measurements.'}"
}
],
"observations": []
},
"notes": "Batch block '40'. Step 1 (epoxidation, RBF with SP-18, AIBN, 2-EH-acrylate feed) has a 2-stage temp/time ramp (40/0.2, 70-75/3.5) plus prose in the 'Other' column carried as procedure events. Step 2 (2 ethyl hexyl acrylate + AIBN) has a 78-82 ramp over 3.5 h and 5.5 h with iodine values IV-42 and IV-27.5. Step 3 charges 'Step - 2 Product' (20 gm) at 55-60 with a feed of Step-I over 25-30 min, and the final product analysis cell 'AV-1.5/SAP-204/HV-183/Amine-285/IV-27.5'. The polysemous Step 2 'A.V.' cell holds 'AV-44.3' (acid value). The printed Remarks column (rightmost) is empty for this block; no date marker line printed. All values copied verbatim; no conversions made.",
"field_confidence": {}
}