Experiments / Batch 76
Batch 76 not OK
04.05.2026 ·
Mr. Mohan Yadav ·
also written as S 9076 · SAW10020626 · BYK 9076 · SAW08020626 · Finalux 108 · NO-P-76 · BYK 9076 STD
Conclusion — verbatim from the source
“Results: Not OK (Gloss and Colour strength inferior).”
pdf/9076 Data for Raven POC project/Application tetsing Report/S 9076 #SAW 10020626 not ok.docx, APPLICATION TEST REPORT
Aim
Application test of dispersing additive S 9076 batch SAW08020626 against reference standard BYK 9076 in Nitrocellulose ink systems (Violet 23, Violet 27, Carbon Black N 330)
Observations
Physical Appearance: Reference Standard BYK 9076 = Amber to yellow viscous liquid; S 9076 = Yellow viscous liquid
Raw materials
| Material | Role |
|---|---|
| BYK 9076 | - |
| S 9076 (Batch No SAW08020626) | - |
| BYK 9076 | - |
| Ink Base – Nitrocellulose Polyurethane | - |
| Violet 23 | - |
| Violet 27 | - |
| Finalux 108 | - |
Reaction conditions (optimized)
other: Re-solubility tested in Ethyl Acetate + Toluene (50:50). Re-solubility Rating: 1 – Fail, 2 – Poor, 3 – Average, 4 – Good, 5 – Excellent
Sample unspecified sample
result
Application test (Nitrocellulose ink, pigment Violet 23)
Grinding < 5 µm; Colour Shade As per Std; Transparency Slightly opaque; Color Strength (%) 100.00; Viscosity (B4 Cup @26°C) 24 s; Adhesion (Tape Test) Pass; Gloss @ 60° 68.1; Re-solubility (Rating) 3; Separation No; Settling No (reference standard: < 5 µm; Reference Std; Reference Std; 100.00; 29 s; Pass; 67.1; 3; No; No)
result
Application test (Nitrocellulose ink, pigment Violet 27)
Grinding < 5 µm; Colour Shade Slightly Bluer; Transparency As per Std; Color Strength (%) 100.00; Viscosity (B4 Cup @26°C) 31 s; Adhesion (Tape Test) Pass; Gloss @ 60° 6.3; Re-solubility (Rating) 3; Separation No; Settling No (reference standard: < 5 µm; Reference Std; Reference Std; 100.00; 27 s; Pass; 8.8; 3; No; No)
result
Application test (Nitrocellulose ink, pigment Carbon Black N 330)
Grinding < 5 µm; Colour Shade As per Std; Transparency As per Std; Color Strength (%) 50-60; Viscosity (B4 Cup @26°C) 40 s; Adhesion (Tape Test) Pass; Gloss @ 60° 17.7; Re-solubility (Rating) 2; Separation No; Settling No (reference standard: < 5 µm; Reference Std; Reference Std; 100.00; 32 s; Pass; 41.9; 3; No; No)
result
Dispersion application test (Violet 23 (Nitrocellulose ink))
result
Dispersion application test (Violet 27 (Nitrocellulose ink))
result
Dispersion application test (Carbon Black N 330 (Nitrocellulose ink))
result
Application test in Ink Base – Nitrocellulose Polyurethane (Violet 23)
Grinding < 5 µm (Ref Std), Colour Shade As per Std, Transparency Opaque (vs Reference Std), Color Strength 98-99 (vs 100.00), Viscosity 23 s (vs 21 s), Adhesion Tape Test Pass, Gloss @ 60° 55.6 (vs 66.4), Re-solubility Rating 2 (vs 4), Separation No, Settling No
vs standard: Gloss inferior (55.6 vs 66.4); Re-solubility inferior (rating 2 Poor vs 4 Good); Colour Strength 98-99 vs 100.00; Transparency Opaque vs Reference Std
result
Application test in Ink Base – Nitrocellulose Polyurethane (Violet 27)
Grinding < 5 µm (Ref Std), Colour Shade As per Std, Transparency Opaque (vs Reference Std), Color Strength 92-93 (vs 100.00), Viscosity 20 s (vs 19 s), Adhesion Tape Test Pass, Gloss @ 60° 8.9 (vs 7.8), Re-solubility Rating 2 (vs 4), Separation No, Settling No
vs standard: Re-solubility inferior (rating 2 Poor vs 4 Good); Colour Strength 92-93 vs 100.00; Transparency Opaque vs Reference Std
IR
16 May 2015
wavenumbers_cm-1: 727.221, 870.465, 931.027, 1014.859, 1111.008, 1251.756, 1347.85, 1297.434, 1373.799, 1458.364, 1555.769, 1540.459, 1643.308, 1698.841, 1733.691, 1838.113, 1829.933, 2017.432, 2008.782, 2341.121, 2473… · transmittance_axis: 5-65 · wavenumber_range_cm-1: 4000-600
· IR BYK 9076 STD.pdf
Sample NO-P-76
13C NMR
30SEP25
· Fine Organics 13C FS PLOT Sample NO-P-76 30SEP25.pdf
1H NMR
30SEP25
· Fine Organics 1H FS PLOT Sample NO-P-76 30SEP25.pdf
13C NMR
30SEP25
· Fine Organics 13C ZOOM1 PLOT Sample NO-P-76 30SEP25.pdf
1H NMR
30SEP25
· Fine Organics 1H ZOOM1 PLOT Sample NO-P-76 30SEP25.pdf
1H NMR
30SEP25
· Fine Organics 1H ZOOM2 PLOT Sample NO-P-76 30SEP25.pdf
13C NMR
30SEP25
· Fine Organics 13C ZOOM2 PLOT Sample NO-P-76 30SEP25.pdf
Sample BYK 9076 STD
IR
· IR BYK 9076 STD.pdf
Test report photos
S 9076 #SAW 10020626 not ok.docx — 2 photos
S 9076 #64 not ok.docx — 2 photos
S 9076 #SAW 08020626 not ok.docx — 2 photos
Where this record comes from
S 9076 #SAW 10020626 not ok.docx
— application testing · linked by a person
S 9076 #SAW 08020626 not ok.docx
— application testing · linked by a person
S 9076 #64 not ok.docx
— application testing · linked by a person
Fine Organics 13C FS PLOT Sample NO-P-76 30SEP25.pdf
— analytical report · linked by a person
Fine Organics 1H FS PLOT Sample NO-P-76 30SEP25.pdf
— analytical report · linked by a person
Fine Organics 13C ZOOM1 PLOT Sample NO-P-76 30SEP25.pdf
— analytical report · linked by a person
Fine Organics 1H ZOOM1 PLOT Sample NO-P-76 30SEP25.pdf
— analytical report · linked by a person
IR BYK 9076 STD.pdf
— analytical report · linked by a person
Fine Organics 1H ZOOM2 PLOT Sample NO-P-76 30SEP25.pdf
— analytical report · linked by a person
Fine Organics 13C ZOOM2 PLOT Sample NO-P-76 30SEP25.pdf
— analytical report · linked by a person
Something wrong on this page? Record a correction
Your correction is permanent: it survives every re-extraction and the field can no longer be changed by the system.
Field-by-field provenance (16 fields) — for auditors
11 extraction fragments · merged 2026-08-25 · 3 human-validated fields
Fix a wrong or missing extraction side-by-side with the original:
qwen-extract--S 9076 SAW 10020626 not ok--s 9076 saw 10020626
qwen-extract--S-9076-#SAW-08020626-not-ok--SAW08020626
qwen-extract--s-9076-64-not-ok--s-9076-64
analytical-name--11239ec3c1b1
analytical-name--16d11e16a4ef
analytical-name--6d431de218a5
analytical-name--e8ccca108c07
analytical-name--ec1d2c8a07f3
analytical-name--fa8baff1289a
analytical-name--feb7aa30bd95
qwen-extract--ir-byk-9076-std--byk-9076
| Field | Source | Extractor | Conf. |
|---|---|---|---|
| date | S 9076 #SAW 10020626 not ok.docx document body, APPLICATION TEST REPORT table | qwen-tasks/extract-fragment.md@unversioned | high |
| scientist | S 9076 #SAW 10020626 not ok.docx document body, APPLICATION TEST REPORT table | qwen-tasks/extract-fragment.md@unversioned | high |
| aim | S 9076 #SAW 10020626 not ok.docx document body, APPLICATION TEST REPORT table | qwen-tasks/extract-fragment.md@unversioned | high |
| conclusion | S 9076 #SAW 10020626 not ok.docx document body, APPLICATION TEST REPORT table | qwen-tasks/extract-fragment.md@unversioned | high |
| materials[0] | S 9076 #SAW 10020626 not ok.docx document body, APPLICATION TEST REPORT table | qwen-tasks/extract-fragment.md@unversioned | high |
| samples[0] | S 9076 #SAW 10020626 not ok.docx document body, APPLICATION TEST REPORT table | qwen-tasks/extract-fragment.md@unversioned | high |
| observations | S 9076 #SAW 10020626 not ok.docx document body, APPLICATION TEST REPORT table | qwen-tasks/extract-fragment.md@unversioned | high |
| outcome | S 9076 #SAW 10020626 not ok.docx document body, APPLICATION TEST REPORT table | qwen-tasks/extract-fragment.md@unversioned | high |
| materials[1] | S 9076 #SAW 08020626 not ok.docx page 1 (report table); page 2 (re-solubility photos) | qwen-tasks/extract-fragment.md@unversioned | high |
| materials[2] | S 9076 #SAW 08020626 not ok.docx page 1 (report table); page 2 (re-solubility photos) | qwen-tasks/extract-fragment.md@unversioned | high |
| materials[3] | S 9076 #64 not ok.docx document (single page) | qwen-tasks/extract-fragment.md@unversioned | high |
| materials[4] | S 9076 #64 not ok.docx document (single page) | qwen-tasks/extract-fragment.md@unversioned | high |
| materials[5] | S 9076 #64 not ok.docx document (single page) | qwen-tasks/extract-fragment.md@unversioned | high |
| materials[6] | S 9076 #64 not ok.docx document (single page) | qwen-tasks/extract-fragment.md@unversioned | high |
| samples[1] | Fine Organics 13C FS PLOT Sample NO-P-76 30SEP25.pdf filename | parse_analytical_names.py@unversioned | high |
| samples[2] | IR BYK 9076 STD.pdf filename | parse_analytical_names.py@unversioned | high |
Raw record JSON
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"project": "9076",
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"S 9076",
"SAW10020626",
"BYK 9076",
"SAW08020626",
"Finalux 108",
"NO-P-76",
"BYK 9076 STD"
],
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"validation": {
"validated_fields": {
"date": {
"validated_by": "FOIL review",
"date": "2026-08-21"
},
"aim": {
"validated_by": "FOIL review",
"date": "2026-08-21"
},
"conclusion": {
"validated_by": "FOIL review",
"date": "2026-08-21"
}
},
"corrections_applied": [
"corr-0011",
"corr-0012",
"corr-0013"
]
},
"date": "04.05.2026",
"scientist": "Mr. Mohan Yadav",
"aim": "Application test of dispersing additive S 9076 batch SAW08020626 against reference standard BYK 9076 in Nitrocellulose ink systems (Violet 23, Violet 27, Carbon Black N 330)",
"conclusion": "Results: Not OK (Gloss and Colour strength inferior).",
"conditions": {
"other": "Re-solubility tested in Ethyl Acetate + Toluene (50:50). Re-solubility Rating: 1 – Fail, 2 – Poor, 3 – Average, 4 – Good, 5 – Excellent"
},
"materials": [
{
"name": "BYK 9076",
"role": "unknown",
"role_verbatim": "Reference Standard"
},
{
"name": "S 9076 (Batch No SAW08020626)",
"role": "unknown",
"notes": "Physical appearance: Yellow viscous liquid",
"role_verbatim": "sample"
},
{
"name": "BYK 9076",
"role": "unknown",
"notes": "Physical appearance: Amber to yellow viscous liquid",
"role_verbatim": "reference_standard"
},
{
"name": "Ink Base – Nitrocellulose Polyurethane",
"role": "unknown",
"role_verbatim": "ink base"
},
{
"name": "Violet 23",
"role": "unknown",
"role_verbatim": "colourant system"
},
{
"name": "Violet 27",
"role": "unknown",
"role_verbatim": "colourant system"
},
{
"name": "Finalux 108",
"role": "unknown",
"role_verbatim": "reference standard for both ink systems"
}
],
"samples": [
{
"name": "S 9076",
"batch_no": "SAW10020626",
"reference_standard": "BYK 9076",
"physical_appearance": "Yellow viscous liquid",
"application_tests": [
{
"test": "Application test",
"system": "Nitrocellulose ink, pigment Violet 23",
"result": "Grinding < 5 µm; Colour Shade As per Std; Transparency Slightly opaque; Color Strength (%) 100.00; Viscosity (B4 Cup @26°C) 24 s; Adhesion (Tape Test) Pass; Gloss @ 60° 68.1; Re-solubility (Rating) 3; Separation No; Settling No (reference standard: < 5 µm; Reference Std; Reference Std; 100.00; 29 s; Pass; 67.1; 3; No; No)"
},
{
"test": "Application test",
"system": "Nitrocellulose ink, pigment Violet 27",
"result": "Grinding < 5 µm; Colour Shade Slightly Bluer; Transparency As per Std; Color Strength (%) 100.00; Viscosity (B4 Cup @26°C) 31 s; Adhesion (Tape Test) Pass; Gloss @ 60° 6.3; Re-solubility (Rating) 3; Separation No; Settling No (reference standard: < 5 µm; Reference Std; Reference Std; 100.00; 27 s; Pass; 8.8; 3; No; No)"
},
{
"test": "Application test",
"system": "Nitrocellulose ink, pigment Carbon Black N 330",
"result": "Grinding < 5 µm; Colour Shade As per Std; Transparency As per Std; Color Strength (%) 50-60; Viscosity (B4 Cup @26°C) 40 s; Adhesion (Tape Test) Pass; Gloss @ 60° 17.7; Re-solubility (Rating) 2; Separation No; Settling No (reference standard: < 5 µm; Reference Std; Reference Std; 100.00; 32 s; Pass; 41.9; 3; No; No)"
},
{
"test": "Dispersion application test",
"system": "Violet 23 (Nitrocellulose ink)",
"results": "{\"grinding_um\": {\"ref_standard\": \"< 5 µm\", \"s_9076\": \"< 5 µm\"}, \"colour_shade\": {\"ref_standard\": \"Reference Std\", \"s_9076\": \"As per Std\"}, \"transparency\": {\"ref_standard\": \"Reference Std\", \"s_9076\": \"Slightly opaque\"}, \"color_strength_pct\": {\"ref_standard\": \"100.00\", \"s_9076\": \"96-97\"}, \"viscosity_b4_cup_26c\": {\"ref_standard\": \"29 s\", \"s_9076\": \"33 s\"}, \"adhesion_tape_test\": {\"ref_standard\": \"Pass\", \"s_9076\": \"Pass\"}, \"gloss_60deg\": {\"ref_standard\": \"67.1\", \"s_9076\": \"63.6\"}, \"re_solubility_rating\": {\"ref_standard\": \"3\", \"s_9076\": \"1\"}, \"separation\": {\"ref_standard\": \"No\", \"s_9076\": \"No\"}, \"settling\": {\"ref_standard\": \"No\", \"s_9076\": \"No\"}}"
},
{
"test": "Dispersion application test",
"system": "Violet 27 (Nitrocellulose ink)",
"results": "{\"grinding_um\": {\"ref_standard\": \"< 5 µm\", \"s_9076\": \"< 5 µm\"}, \"colour_shade\": {\"ref_standard\": \"Reference Std\", \"s_9076\": \"As per Std\"}, \"transparency\": {\"ref_standard\": \"Reference Std\", \"s_9076\": \"As per Std\"}, \"color_strength_pct\": {\"ref_standard\": \"100.00\", \"s_9076\": \"100.00\"}, \"viscosity_b4_cup_26c\": {\"ref_standard\": \"27 s\", \"s_9076\": \"29 s\"}, \"adhesion_tape_test\": {\"ref_standard\": \"Pass\", \"s_9076\": \"Pass\"}, \"gloss_60deg\": {\"ref_standard\": \"8.8\", \"s_9076\": \"8.5\"}, \"re_solubility_rating\": {\"ref_standard\": \"3\", \"s_9076\": \"3\"}, \"separation\": {\"ref_standard\": \"No\", \"s_9076\": \"No\"}, \"settling\": {\"ref_standard\": \"No\", \"s_9076\": \"No\"}}"
},
{
"test": "Dispersion application test",
"system": "Carbon Black N 330 (Nitrocellulose ink)",
"results": "{\"grinding_um\": {\"ref_standard\": \"< 5 µm\", \"s_9076\": \"< 5 µm\"}, \"colour_shade\": {\"ref_standard\": \"Reference Std\", \"s_9076\": \"As per Std\"}, \"transparency\": {\"ref_standard\": \"Reference Std\", \"s_9076\": \"As per Std\"}, \"color_strength_pct\": {\"ref_standard\": \"100.00\", \"s_9076\": \"100.00\"}, \"viscosity_b4_cup_26c\": {\"ref_standard\": \"32 s\", \"s_9076\": \"37 s\"}, \"adhesion_tape_test\": {\"ref_standard\": \"Pass\", \"s_9076\": \"Pass\"}, \"gloss_60deg\": {\"ref_standard\": \"41.9\", \"s_9076\": \"42.3\"}, \"re_solubility_rating\": {\"ref_standard\": \"3\", \"s_9076\": \"1\"}, \"separation\": {\"ref_standard\": \"No\", \"s_9076\": \"No\"}, \"settling\": {\"ref_standard\": \"No\", \"s_9076\": \"No\"}}"
},
{
"test": "Application test in Ink Base – Nitrocellulose Polyurethane",
"system": "Violet 23",
"reference": "BYK 9076 / Finalux 108",
"conditions": "Re-solubility tested in Ethyl Acetate + Toluene (50:50); Viscosity B4 Cup @26°C; Gloss @ 60°",
"result": "Grinding < 5 µm (Ref Std), Colour Shade As per Std, Transparency Opaque (vs Reference Std), Color Strength 98-99 (vs 100.00), Viscosity 23 s (vs 21 s), Adhesion Tape Test Pass, Gloss @ 60° 55.6 (vs 66.4), Re-solubility Rating 2 (vs 4), Separation No, Settling No",
"vs_reference": "Gloss inferior (55.6 vs 66.4); Re-solubility inferior (rating 2 Poor vs 4 Good); Colour Strength 98-99 vs 100.00; Transparency Opaque vs Reference Std"
},
{
"test": "Application test in Ink Base – Nitrocellulose Polyurethane",
"system": "Violet 27",
"reference": "BYK 9076 / Finalux 108",
"conditions": "Re-solubility tested in Ethyl Acetate + Toluene (50:50); Viscosity B4 Cup @26°C; Gloss @ 60°",
"result": "Grinding < 5 µm (Ref Std), Colour Shade As per Std, Transparency Opaque (vs Reference Std), Color Strength 92-93 (vs 100.00), Viscosity 20 s (vs 19 s), Adhesion Tape Test Pass, Gloss @ 60° 8.9 (vs 7.8), Re-solubility Rating 2 (vs 4), Separation No, Settling No",
"vs_reference": "Re-solubility inferior (rating 2 Poor vs 4 Good); Colour Strength 92-93 vs 100.00; Transparency Opaque vs Reference Std"
}
],
"sample_id": "unspecified sample",
"analytical": [
{
"technique": "IR",
"date": "16 May 2015",
"file": "IR BYK 9076 STD.pdf",
"printed_result": "{\"wavenumbers_cm-1\": [727.221, 870.465, 931.027, 1014.859, 1111.008, 1251.756, 1347.85, 1297.434, 1373.799, 1458.364, 1555.769, 1540.459, 1643.308, 1698.841, 1733.691, 1838.113, 1829.933, 2017.432, 2008.782, 2341.121, 2473.474, 2456.367, 2869.717, 2929.889, 2969.138, 3488.439, 3583.659], \"transmittance_axis\": \"5-65\", \"wavenumber_range_cm-1\": \"4000-600\"}"
}
]
},
{
"sample_id": "NO-P-76",
"analytical": [
{
"technique": "13C NMR",
"file": "Analytical Report/NMR/9076/Fine Organics 13C FS PLOT Sample NO-P-76 30SEP25.pdf",
"date": "30SEP25"
},
{
"technique": "1H NMR",
"file": "Analytical Report/NMR/9076/Fine Organics 1H FS PLOT Sample NO-P-76 30SEP25.pdf",
"date": "30SEP25"
},
{
"technique": "13C NMR",
"file": "Analytical Report/NMR/9076/Fine Organics 13C ZOOM1 PLOT Sample NO-P-76 30SEP25.pdf",
"date": "30SEP25"
},
{
"technique": "1H NMR",
"file": "Analytical Report/NMR/9076/Fine Organics 1H ZOOM1 PLOT Sample NO-P-76 30SEP25.pdf",
"date": "30SEP25"
},
{
"technique": "1H NMR",
"file": "Analytical Report/NMR/9076/Fine Organics 1H ZOOM2 PLOT Sample NO-P-76 30SEP25.pdf",
"date": "30SEP25"
},
{
"technique": "13C NMR",
"file": "Analytical Report/NMR/9076/Fine Organics 13C ZOOM2 PLOT Sample NO-P-76 30SEP25.pdf",
"date": "30SEP25"
}
]
},
{
"sample_id": "BYK 9076 STD",
"analytical": [
{
"technique": "IR",
"file": "Analytical Report/IR/IR BYK 9076 STD.pdf"
}
]
}
],
"observations": "Physical Appearance: Reference Standard BYK 9076 = Amber to yellow viscous liquid; S 9076 = Yellow viscous liquid",
"outcome": {
"status": "not ok",
"basis": "Results: Not OK (Gloss and Colour strength inferior).",
"citation": "pdf/9076 Data for Raven POC project/Application tetsing Report/S 9076 #SAW 10020626 not ok.docx, APPLICATION TEST REPORT"
}
}