Observations
Expt Table remarks: Tested sample and found good results likely resolubility/ tinting strenghth/ gloss etc. with respect to reference product. AV-37.6 Amine- 35.3
Raw materials (collected from the per-step charges)
| Step | Material | Role |
|---|---|---|
| 1 | Vicasurf 1010 (HV-115-120) | reactant |
| 1 | Phosphorous pentaoxide | reactant |
| 2 | Epomine SP- 018 | reactant |
| 2 | 2 ethyl hexyl acrylate | reactant |
| 3 | Amine-224 | reactant |
| 3 | Step- 1 product | intermediate |
| 3 | Step - 2 Product | intermediate |
Process
| Step | Conditions | Charged | What happened | Results |
|---|---|---|---|---|
|
Step 1
28112025 9076 Expt Table 2025.xls
|
temperature: 60 then 80 (multi-line cell, positional ramp pairing)atmosphere: N2time_h: 1 then 4 |
Vicasurf 1010 (HV-115-120) Phosphorous pentaoxide
|
A.V. cell '33' not labelled (AV vs amine value undetermined).
—
|
|
|
Step 2
28112025 9076 Expt Table 2025.xls
|
temperature: 68 then 78 (multi-line cell, positional ramp pairing)atmosphere: N2time_h: 2 then 4 |
Epomine SP- 018 2 ethyl hexyl acrylate
|
— | — |
|
Step 3
28112025 9076 Expt Table 2025.xls
|
temperature: 160 (single value in multi-line cell; second line blank)atmosphere: N2time_h: 1 |
Amine-224 Step- 1 product Step - 2 Product
|
Amine-224 qty cell empty. The value '40' sits in the Step 3 Qty (g) column with no matching material name row; recorded here and not force-fitted to any step.
—
|
— |
No test results linked to this batch yet.
Where this record comes from
28112025 9076 Expt Table 2025.xls
— researcher summary (cross-check)
Something wrong on this page? Record a correction
Your correction is permanent: it survives every re-extraction and the field can no longer be changed by the system.
Field-by-field provenance (5 fields) — for auditors
1 extraction fragments · merged 2026-08-25 · 0 human-validated fields
Fix a wrong or missing extraction side-by-side with the original:
expt-block--14
| Field | Source | Extractor | Conf. |
|---|---|---|---|
| record_type | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '14' | qwen-tasks/extract-expt-block.md@unversioned | high |
| process_steps[0] | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '14' | qwen-tasks/extract-expt-block.md@unversioned | high |
| process_steps[1] | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '14' | qwen-tasks/extract-expt-block.md@unversioned | high |
| process_steps[2] | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '14' | qwen-tasks/extract-expt-block.md@unversioned | high |
| observations | 28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '14' | qwen-tasks/extract-expt-block.md@unversioned | high |
Raw record JSON
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"validation": {
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"record_type": "synthesis",
"process_steps": [
{
"step": 1,
"materials": [
{
"name": "Vicasurf 1010 (HV-115-120)",
"qty_g": 300,
"role": "reactant"
},
{
"name": "Phosphorous pentaoxide",
"qty_g": 9.5,
"role": "reactant"
}
],
"procedure": [
{
"seq": 1,
"temperature": "60",
"time_h": "1",
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},
{
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"temperature": "80",
"time_h": "4",
"verbatim": "80 / 4"
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"conditions": {
"temperature": "60 then 80 (multi-line cell, positional ramp pairing)",
"atmosphere": "N2",
"time_h": "1 then 4"
},
"results": [
{
"parameter": "unlabelled",
"value": "33",
"verbatim": "A.V. column: 33"
}
],
"remarks": "A.V. cell '33' not labelled (AV vs amine value undetermined)."
},
{
"step": 2,
"materials": [
{
"name": " Epomine SP- 018",
"qty_g": 105,
"role": "reactant"
},
{
"name": "2 ethyl hexyl acrylate",
"qty_g": 245,
"role": "reactant"
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],
"procedure": [
{
"seq": 1,
"temperature": "68",
"time_h": "2",
"verbatim": "68 / 2"
},
{
"seq": 2,
"temperature": "78",
"time_h": "4",
"verbatim": "78 / 4"
}
],
"conditions": {
"temperature": "68 then 78 (multi-line cell, positional ramp pairing)",
"atmosphere": "N2",
"time_h": "2 then 4"
},
"results": []
},
{
"step": 3,
"materials": [
{
"name": "Amine-224",
"role": "reactant"
},
{
"name": "Step- 1 product",
"qty_g": 80,
"role": "intermediate"
},
{
"name": "Step - 2 Product",
"qty_g": 20,
"role": "intermediate"
}
],
"procedure": [
{
"seq": 1,
"temperature": "160",
"time_h": "1",
"verbatim": "160 / 1"
},
{
"seq": 2,
"verbatim": "40 (Qty col); N2 (Vac/N2 col)"
}
],
"conditions": {
"temperature": "160 (single value in multi-line cell; second line blank)",
"atmosphere": "N2",
"time_h": "1"
},
"results": [],
"remarks": "Amine-224 qty cell empty. The value '40' sits in the Step 3 Qty (g) column with no matching material name row; recorded here and not force-fitted to any step."
}
],
"observations": "Expt Table remarks: Tested sample and found good results likely resolubility/ tinting strenghth/ gloss etc. with respect to reference product.\nAV-37.6 \nAmine- 35.3"
}