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Experiments / Batch 11

Batch 11 no result yet

also written as 11
Observations

Expt Table remarks: AV-36.7 Expt Table remarks: Amine value- 37

Raw materials (collected from the per-step charges)
StepMaterialRole
1Vicasurf -1010 (HV-115-120)-
1Phosphorous pentaoxide-
2Epomine SP- 018-
22 ethyl hexyl acrylate-
3Step- 1 product (80)intermediate
3Step - 2 Product (20)intermediate
Process
Step Conditions Charged What happened Results
Step 1
28112025 9076 Expt Table 2025.xls
temperature: 40 / 55 / 75atmosphere: N2time_h: 0.15 / 0.5 / 1 hr- 2 hr
Vicasurf -1010 (HV-115-120)
Phosphorous pentaoxide
acid_value 38
Step 2
28112025 9076 Expt Table 2025.xls
temperature: 68 / 78atmosphere: N2time_h: 2 / 4
Epomine SP- 018
2 ethyl hexyl acrylate
acid_value 257
Step 3
28112025 9076 Expt Table 2025.xls
temperature: 60 / 65atmosphere: N2time_h: 1 / 3
Step- 1 product (80)
Step - 2 Product (20)
acid_value 36.7 amine_value 37

No test results linked to this batch yet.

Where this record comes from
28112025 9076 Expt Table 2025.xls — researcher summary (cross-check)
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Field-by-field provenance (4 fields) — for auditors
1 extraction fragments · merged 2026-08-25 · 0 human-validated fields
Fix a wrong or missing extraction side-by-side with the original: expt-block--11
FieldSourceExtractorConf.
process_steps[0]28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '11', csv rows 38-40 qwen-tasks/extract-expt-block.md@unversionedhigh
process_steps[1]28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '11', csv rows 38-40 qwen-tasks/extract-expt-block.md@unversionedhigh
process_steps[2]28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '11', csv rows 38-40 qwen-tasks/extract-expt-block.md@unversionedhigh
observations28112025 9076 Expt Table 2025.xls sheet 9076_Experiments, batch block '11', csv rows 38-40 qwen-tasks/extract-expt-block.md@unversionedhigh
Raw record JSON
{
  "record_id": "exp-9076-011",
  "project": "9076",
  "aliases": [
    "11"
  ],
  "provenance": {
    "fragments": [
      "expt-block--11"
    ],
    "field_provenance": {
      "process_steps[0]": {
        "source_file": "docs/Project Expt Report/28112025  9076 Expt Table 2025.xls",
        "extractor": "qwen-tasks/extract-expt-block.md",
        "extractor_version": "unversioned",
        "extracted_date": "2026-08-19",
        "locator": "sheet 9076_Experiments, batch block '11', csv rows 38-40",
        "human_checked": true
      },
      "process_steps[1]": {
        "source_file": "docs/Project Expt Report/28112025  9076 Expt Table 2025.xls",
        "extractor": "qwen-tasks/extract-expt-block.md",
        "extractor_version": "unversioned",
        "extracted_date": "2026-08-19",
        "locator": "sheet 9076_Experiments, batch block '11', csv rows 38-40",
        "human_checked": true
      },
      "process_steps[2]": {
        "source_file": "docs/Project Expt Report/28112025  9076 Expt Table 2025.xls",
        "extractor": "qwen-tasks/extract-expt-block.md",
        "extractor_version": "unversioned",
        "extracted_date": "2026-08-19",
        "locator": "sheet 9076_Experiments, batch block '11', csv rows 38-40",
        "human_checked": true
      },
      "observations": {
        "source_file": "docs/Project Expt Report/28112025  9076 Expt Table 2025.xls",
        "extractor": "qwen-tasks/extract-expt-block.md",
        "extractor_version": "unversioned",
        "extracted_date": "2026-08-19",
        "locator": "sheet 9076_Experiments, batch block '11', csv rows 38-40",
        "human_checked": true
      }
    },
    "last_merged": "2026-08-25"
  },
  "documents": [
    {
      "file": "docs/Project Expt Report/28112025  9076 Expt Table 2025.xls",
      "role": "summary_table",
      "link_basis": "alias match: 11",
      "link_status": "rule"
    }
  ],
  "validation": {
    "validated_fields": {},
    "corrections_applied": []
  },
  "process_steps": [
    {
      "step": 1,
      "materials": [
        {
          "name": "Vicasurf -1010 (HV-115-120)",
          "qty_g": "300",
          "role": "unknown",
          "role_verbatim": "raw_material"
        },
        {
          "name": "Phosphorous pentaoxide",
          "qty_g": "10.5",
          "role": "unknown",
          "role_verbatim": "raw_material"
        }
      ],
      "procedure": [
        {
          "seq": 1,
          "temperature": "40",
          "time_h": "0.15",
          "verbatim": "40 / 0.15"
        },
        {
          "seq": 2,
          "temperature": "55",
          "time_h": "0.5",
          "atmosphere": "N2",
          "verbatim": "55 / 0.5 / N2"
        },
        {
          "seq": 3,
          "temperature": "75",
          "time_h": "1 hr- 2 hr",
          "verbatim": "75 / 1 hr- 2 hr"
        }
      ],
      "conditions": {
        "temperature": "40 / 55 / 75",
        "atmosphere": "N2",
        "time_h": "0.15 / 0.5 / 1 hr- 2 hr"
      },
      "results": [
        {
          "parameter": "acid_value",
          "value": "38",
          "verbatim": "A.V. cell: 38"
        }
      ],
      "remarks": ""
    },
    {
      "step": 2,
      "materials": [
        {
          "name": "Epomine SP- 018",
          "qty_g": "105",
          "role": "unknown",
          "role_verbatim": "raw_material"
        },
        {
          "name": "2 ethyl hexyl acrylate",
          "qty_g": "245",
          "role": "unknown",
          "role_verbatim": "raw_material"
        }
      ],
      "procedure": [
        {
          "seq": 1,
          "temperature": "68",
          "time_h": "2",
          "verbatim": "68 / 2"
        },
        {
          "seq": 2,
          "temperature": "78",
          "time_h": "4",
          "atmosphere": "N2",
          "verbatim": "78 / 4 / N2"
        }
      ],
      "conditions": {
        "temperature": "68 / 78",
        "atmosphere": "N2",
        "time_h": "2 / 4"
      },
      "results": [
        {
          "parameter": "acid_value",
          "value": "257",
          "verbatim": "A.V. cell: 257"
        }
      ],
      "remarks": ""
    },
    {
      "step": 3,
      "materials": [
        {
          "name": "Step-  1 product  (80)",
          "qty_g": "160",
          "role": "intermediate"
        },
        {
          "name": "Step -  2 Product (20)",
          "qty_g": "40",
          "role": "intermediate"
        }
      ],
      "procedure": [
        {
          "seq": 1,
          "temperature": "60",
          "time_h": "1",
          "verbatim": "60 / 1"
        },
        {
          "seq": 2,
          "temperature": "65",
          "time_h": "3",
          "atmosphere": "N2",
          "verbatim": "65 / 3 / N2"
        }
      ],
      "conditions": {
        "temperature": "60 / 65",
        "atmosphere": "N2",
        "time_h": "1 / 3"
      },
      "results": [
        {
          "parameter": "acid_value",
          "value": "36.7",
          "verbatim": "AV-36.7"
        },
        {
          "parameter": "amine_value",
          "value": "37",
          "verbatim": "Amine value- 37"
        }
      ],
      "remarks": ""
    }
  ],
  "observations": "Expt Table remarks: AV-36.7\nExpt Table remarks: Amine value- 37"
}