Extracted text · 9076 ppt.md
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# 9076 ppt.pptx
## Slide 1
R&D projects review meeting
Feb 2023
## Slide 2
Product:- 9076
Wetting and dispersing additive for solvent-borne and solvent-free coatings, adhesives, PVC plastisols, ambient curing resin systems, and color masterbatches for thermoplastics.
Particularly recommended for carbon black pigments. Prevents separation and improves the fiber wetting in SMC/BMC formulations.
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## Slide 3
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## Slide 4
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## Slide 5
Product:- 9076
Test
Unit
P-9076
Appearance
Visual
Viscous yellowish liquid
Acid Value
mg OH / g
40
Sap Value
mgKOH g
45
Amine value
mgKOH g
31
OH Value
mgKOH/ g
35
Iodine Value
gm/100g
4.15
LOD @150C, 60 min
%
12
P- content
%
0.75%
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## Slide 6
R&D projects review meeting
June 2023
## Slide 7
Product:- 9076
Test
Unit
P-9076
LBN # 11
Appearance
Visual
Viscous yellowish liquid
Viscous yellowish liquid
Acid Value
mg OH / g
40
38.5
Sap Value
mgKOH g
45
64
Amine value
mgKOH g
31
42
OH Value
mgKOH/ g
35
80
Iodine Value
gm/100g
4.15
0.9
LOD @150C, 60 min
%
12 (Toluene/Methoxy propyl acetate, 2 ethyl hexanol confirmed by GC/MS)
8.2
P- content
%
0.75%
0.78%
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## Slide 8
Amine + 2 ethyl hexyl acrylate
Product
Intermediate 1
Process B. NO. 11
Current Status:- Lab application approved , planning for 1 kg sample .
Heating 68-78 deg C
Intermediate 2
Heating 45- 80 deg C
EO-PO (HV-115-120)+ Phosphorous pentaoxide
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## Slide 9
Application test – B. No. 11
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## Slide 10
Application test – B. No. 11
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## Slide 11
R&D projects review meeting
July 2023
## Slide 12
Product:- 9076
Wetting and dispersing additive for solvent-borne and solvent-free coatings, adhesives, PVC plastisols, ambient curing resin systems, and color masterbatches for thermoplastics.
Recommended for carbon black pigments- improves fiber wetting in SMC/BMC formulations.
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## Slide 13
Product:- 9076
Test
Unit
P-9076
LBN # 11
#LBN 12
Appearance
Visual
Viscous yellowish liquid
Viscous yellowish liquid
Viscous yellowish liquid
Acid Value
mg OH / g
40
38.5
42
Sap Value
mgKOH g
45
64
70
Amine value
mgKOH g
31
42
35
OH Value
mgKOH/ g
35
80
86
Iodine Value
gm/100g
4.15
0.9
0.7
LOD @150C, 60 min
%
12 (Toluene/Methoxy propyl acetate, 2 ethyl hexanol confirmed by GC/MS)
8.2
8.28
P- content
%
0.75%
0.78%
0.77%
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## Slide 14
Epomine 018 + 2 ethyl hexyl acrylate
Product
Intermediate 1
Process B. NO. 11
Current Status:- Lab application approved , planning for 1 kg sample .
Heating 68-78 deg C
Intermediate 2
Heating 45- 80 deg C
Vicasurf 1010 (HV-115-120)+ Phosphorous pentaoxide
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## Slide 15
Application test – B. No. 11
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## Slide 16
Application test – B. No. 11
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## Slide 17
R&D projects review meeting
August 2023
## Slide 18
Product:- 9076
Wetting and dispersing additive for solvent-borne and solvent-free coatings, adhesives, PVC plastisols, ambient curing resin systems, and color masterbatches for thermoplastics.
Recommended for carbon black pigments- improves fiber wetting in SMC/BMC formulations.
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## Slide 19
Product:- 9076
Test
Unit
P-9076
LBN # 11
#LBN 12
Appearance
Visual
Viscous yellowish liquid
Viscous yellowish liquid
Viscous yellowish liquid
Acid Value
mg OH / g
40
38.5
42
Sap Value
mgKOH g
45
64
70
Amine value
mgKOH g
31
42
35
OH Value
mgKOH/ g
35
80
86
Iodine Value
gm/100g
4.15
0.9
0.7
LOD @150C, 60 min
%
12 (Toluene/Methoxy propyl acetate, 2 ethyl hexanol confirmed by GC/MS)
8.2
8.28
P- content
%
0.75%
0.78%
0.77%
Current Status:- Lab application approved , planning / Fine tuning for black pigment
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## Slide 20
Amine + 2 ethyl hexyl acrylate
Product
Intermediate 1
Process
Intermediate 2
Vicasurf 1010 + Phosphotising agent
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## Slide 21
R&D projects review meeting
September 2023
## Slide 22
R&D Ref No
Date
19.08.2023
No. Samples
01
Product Name
9076 (New Sample) 15.8.23
Manufacturer
Received from
Mr. Nilesh Pawar
Analyzed by
Pramod
Test
Unit
-9076 ( Old sample )
-9076 New Sample Aug 2023
Appearance
Visual
Viscous yellowish liquid
Viscous yellowish liquid
Acid Value
mg OH / g
40
45
Sap Value
mgKOH g
45
67.1
Amine value
mgKOH g
31
32
OH Value
mgKOH/ g
35
65
Iodine Value
gm/100g
4.15
0.8
LOD @150C, 60 min
%
12 (Toluene/Methoxy propyl acetate, 2 ethyl hexanol confirmed by GC/MS)
5.8%( Methoxy propyl acetate, 2 ethyl hexanol - By head space )
P- content
%
0.75%
1.71%
EO/PO ( By HI method)
%
41.56
56.18%
Observations: Based on analysis product is Amine neutralized phosphate EO/PO ester.
INTERNAL TEST REPORT [MARKET / COMPETITION SAMPLE]
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## Slide 23
R&D projects review meeting
December 2023
## Slide 24
Finasperse 1976
Lab batches done under testing
Sr.No
Test
Unit
9076 (Ref)
LBN-21
LBN-22
LBN -23
1
Appearance
Visual
Viscous yellowish liquid
Viscous yellowish liquid
(SurfolR-1400)
Viscous yellowish liquid
(BEP-1450)
Viscous yellowish liquid(SurfolR-1400)
2
Acid Value
mg OH / g
43.2
42.56
43.7
42.67
3
Sap Value
mgKOH g
54
67.44
78.51
63.50
4
Amine value
mgKOH g
30.1
40.56
32.55
39.8
5
OH Value
mgKOH/ g
65
58.9
67.7
55.32
6
Iodine Value
gm/100g
9.3
8.2
15.5
7.22
Sample submitted to TACO for application test.
## Slide 25
-9076
LBN- 21A
-9076
LBN- 21B
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## Slide 26
R&D projects review meeting
February- 2023
## Slide 27
Product Name
9076/ LBN 24 Comparison
Test
Unit
9076
LBN -24A
LBN -24B
LBN -24C
LBN -24CR
LBN -24-CR2
Appearance
Visual
Viscous yellowish liquid
Viscous yellowish liquid
Viscous yellowish liquid
Viscous yellowish liquid
Viscous yellowish liquid
Viscous yellowish liquid
Acid Value
mg OH / g
43.2
53
37.97
35.56
35.43
35.25
Sap Value
mgKOH g
54
85.9
82.5
84.7
82.5
83.6
Amine value
mgKOH g
30.1
29.5
27.8
29.79
31.1
30.9
OH Value
mgKOH/ g
65
65
83
70.4
66.1
65
Iodine Value
gm/100g
9.3
6.2
5.8
7.1
6.7
7.5
Lab batch analysis details : 9076
## Slide 28
LBN No.
Parameters /Pigments
Black N 330
Red 57:1
Blue 15:3
Red 146
Red 53:1
Red 48:2
Orange 13
Yellow
White 6
Violet 23
Violet 27
Green 7
24CR
Resolubility
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
4% weaker
5 % weaker
Pass
Strength
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Fail
Pass
Inferior
24C
Resolubility
Pass
Pass
Pass
---
---
---
---
---
---
---
---
Pass
Strength
Pass
Pass
Pass
---
---
---
---
---
---
---
---
Pass
24B
Resolubility
Pass
Pass
Pass
---
---
---
---
---
---
---
---
5 % weaker
Strength
Pass
Pass
Pass
---
---
---
---
---
---
---
---
Inferior
24 A
Resolubility
Pass
Pass
---
---
---
---
---
---
---
---
---
3 % weaker
Strength
Pass
Pass
---
---
---
---
---
---
---
---
---
Pass
Application test: 9076
## Slide 29
Thank you
## Slide 30
R&D projects review meeting
April- 2023
## Slide 31
Application test: 9076
(Butanol EO-PO based Batches)
Parameters
Black N 330
Red 57:1
Blue 15:3
Red 146
Red 53:1
Red 48:2
Orange 13
Yellow
White 6
Violet 23
Violet 27
Green 7
LBN
Resolubility
Pass
Pass
Pass
Pass
24C
Strength
Pass
Pass
Pass
Pass
Gloss
Pass
Pass
Pass
Pass
Shade
Pass
Pass
Pass
Slight yellower
Transparency
Pass
Pass
Pass
Slight opaque
LBN
Resolubility
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Fail
Pass
Slight Inferior
24C (R )
Strength
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Weaker
Weaker
Pass
Gloss
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Shade
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Slight inferior
Transparency
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Opaque
Opaque
Slight opaque
LBN
Resolubility
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Fail
24C (R-2)
Strength
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Slight weaker
Pass
Gloss
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Shade
Pass
Pass
Pass
Pass
Yellower
Pass
yellower
Redder
Pass
Pass
Redder
Slight yellower
Transparency
Pass
Pass
Pass
Pass
Pass
Pass
Pass
Opaque
Pass
Pass
Opaque
Pass
LBN
Resolubility
Pass
Fail
Pass
Pass
24C (I)
Strength
Pass
Pass
Pass
Pass
Gloss
Pass
Slight Inferior
Pass
Slight less
Shade
Pass
Pass
Pass
Slight yellower
Transparency
Pass
Opaque
Pass
Slight opaque
LBN
Resolubility
Slightly inferior
Pass
Pass
Pass
Pass
Pass
Fail
26 A
Strength
Pass
Pass
Pass
Pass
slight weaker
Pass
Pass
Gloss
Pass
Inferior
Pass
Pass
Slight poor
Slight poor
Slight poor
Shade
Pass
Pass
Pass
Slight yellower
Pass
Pass
Pass
Transparency
Pass
Pass
Pass
Pass
Opaque
Pass
Pass
LBN
Resolubility
Slightly inferior
Pass
Pass
Pass
26 B
Strength
Pass
Pass
Slight inferior
Pass
Gloss
Pass
Pass
Pass
Pass
Shade
Pass
Pass
Pass
Pass
Transparency
Pass
Pass
Pass
Pass
## Slide 32
9076 equivalent trial batch Data
LBN
AV
IV
%P Content
SAP
Amine value
LBN -24C
35.56
7.1
1.43
84.7
29.79
LBN -24CR
35.43
6.7
1.36
82.5
31.1
LBN -24-CR2
35.25
7.5
1.401
83.6
30.9
LBN -25 A
36.86
7.1
1.15
74.18
40.7
LBN -25 B
36.86
7.5
1.138
74.1
35.92
LBN -26 A
35.42
6.2
1.305
67.07
38.5
LBN -26 B
35.01
7.5
1.308
71.2
36.34
Analysis Details
## Slide 33
Shade
Resolubility
Gloss
Strength
Transparency
Batch No.
LBN 27 A
Pigmnets
Green
Yellower than std
Pass
31.1/25.9
Pass
Slight opaque
Violet
Redder than std
Pass
63.8/56.3
Pass
Slight opaque
Batch No.
LBN 27 B
Pigmnets
Green
Yellower than std
Pass
31.1/25.9
Pass
Slight opaque
Violet
Redder than std
Pass
63.8/56.3
Pass
Slight opaque
Batch No.
LBN 27 C
Pigmnets
Green
Yellower than std
Pass
31.1/24.9
Pass
Slight opaque
Violet
Redder than std
Fail
63.1/55
Pass
Slight opaque
Batch No.
LBN 27 D
Pigmnets
Green
Yellower than std
Pass
30.3/28.2
Pass
Slight opaque
Violet
Redder than std
Pass
60.8/50.3
Pass
Slight opaque
Batch No.
LBN 27 E
Pigmnets
Green
Pass
Fail
30.5/30.1
Pass
Pass
Violet
Pass
Fail
69.9/67.9
Pass
Pass
Application test: 9076
(Vicasurf-1010 based Batches)
## Slide 34
Product Name
9076/ LBN 27Comparison
Test
Unit
9076
LBN -27A
LBN -27B
LBN -27C
LBN -27D
LBN -27 E
Appearance
Visual
Viscous yellowish liquid
Viscous yellowish liquid
Viscous yellowish liquid
Viscous yellowish liquid
Viscous yellowish liquid
Viscous yellowish liquid
Acid Value
mg OH / g
43.2
36.6
33.7
29.1
33.1
29.98
Sap Value
mgKOH g
54
59.4
63.2
62.3
56.8
53.9
Amine value
mgKOH g
30.1
40.1
27.8
29.79
31.1
30.9
OH Value
mgKOH/ g
65
71.92
77.4
84.3
78
82.21
Iodine Value
gm/100g
9.3
5.5
5.81
6.87
4.5
Analysis Details
## Slide 35
R&D projects review meeting
June- 2023
## Slide 36
Product Name
9076/ LBN 28 A-B/ LBN 29 A-B Comparison
Test
Unit
9076
LBN -28 A
LBN -28 -B
LBN -28C
LBN -29A
LBN- 29B
Appearance
Visual
Viscous yellowish liquid
Viscous yellowish liquid
Viscous yellowish liquid
Viscous yellowish liquid
Viscous yellowish liquid
Viscous yellowish liquid
Acid Value
mg OH / g
43.2
29.2
32.01
28.2
25.22
26.62
Sap Value
mgKOH g
54
72.7
62.1
61.5
59.83
60.5
Amine value
mgKOH g
30.1
42.5
41
43.5
45.1
42.7
OH Value
mgKOH/ g
65
66.71
64.2
82
67.2
61.5
Iodine Value
gm/100g
9.3
8.5
7.5
6.15
6.4
5.8
Analysis Details
## Slide 37
R&D projects review meeting
August- 2023
## Slide 38
Analysis Details
Product Name
9076/ LBN 29 A/B/D / 30Comparison
Test
Unit
9076
LBN -29A
LBN- 29B
LBN- 29D
LBN 30
Appearance
Visual
Viscous yellowish liquid
Viscous yellowish liquid
Viscous yellowish liquid
Viscous yellowish liquid
Viscous yellowish liquid
Acid Value
mg O