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← Lab Batch 24A.pdf ·next unchecked fragment →
Original · Lab Batch 24A.pdf
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Experiment: exp-9076-024A
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aim
highTo develop product equivalent to reference product
temperature
high60-65
atmosphere
highN2
time
high4h
Materials high
| # | sr_no | name | source | quantity | unit | purity_pct | moles | molar_ratio | molecular_wt |
|---|---|---|---|---|---|---|---|---|---|
| 0 | 1 | Vicaspin LUB 1010 (R225100845) Bu- EO-PO HV-62.3/ MW-900 | Viswaat | 170.0 | gms | 900 | 0.19 | 1.0 | — |
| 1 | 2 | P2O5 | Commercial | 7.655 | gms | — | 0.054 | 0.28 | — |
| 2 | 3 | Epomine SP-012 | Nippon | 37.3 | gms | 100 | — | — | — |
| 3 | 4 | 2 ethyl hexyl acrylate | — | 59.5 | gms | 100 | 0.32 | — | 184.3 |
| 4 | 5 | AIBN | — | 0.79 | gms | — | — | — | — |
| 5 | 6 | Step- B reaction mass (20%) | — | 38.2 | gms | — | — | — | — |
| 6 | 7 | Step- A product | — | 164.9 | gms | — | — | — | — |
Process steps high
| Step | Charged | What happened | Results | ||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
|
Step 1
time 0.5 temperature 50-55
|
— |
|
— | ||||||||||
| other fields step_id Step- A | |||||||||||||
|
Step 2
time 3 temperature 45-50
|
— |
|
— | ||||||||||
| other fields step_id Step-B | |||||||||||||
|
Step 3
time 1-2 temperature 65-70
|
— |
|
— | ||||||||||
| other fields step_id Step-C | |||||||||||||
[
{
"procedure": [
{
"action": "To main reactor added Vicaspin LUB 1010 (R225100845) Bu- EO-PO HV-62.3/ MW-900 under stirring and nitrogen atmosphere temp. 40 deg increased temp slowly with addition of P2O5"
}
],
"remarks": "viscous clear mass",
"step": 1,
"step_id": "Step- A",
"temperature": "50-55",
"time": "0.5"
},
{
"procedure": [
{
"action": "To main reactor added Epomine SP-012- reaction mass held with slow addition of 2 ethyl hexyl acrylate, checked free acid at interval"
}
],
"remarks": "AV-45.0, free acid 0.5",
"step": 2,
"step_id": "Step-B",
"temperature": "45-50",
"time": "3"
},
{
"procedure": [
{
"action": "To main reactor added Step- B reaction mass (20%) and Step- A product, mixed till uniform"
}
],
"remarks": "AV 43.2 Amine 30.0",
"step": 3,
"step_id": "Step-C",
"temperature": "65-70",
"time": "1-2"
}
]
More actions — correct a value · link · ignore
Raw fragment JSON
{
"fragment_id": "qwen-extract--lab-batch-24a--lbn-24a",
"source_file": "pdf/9076 Data for Raven POC project/Old ELN/Lab Batch 24A.pdf",
"derived_from": "ocr/Lab Batch 24A",
"locator": "Page 1",
"extractor": "qwen-tasks/extract-fragment.md",
"target_aliases": [
"LBN 24A",
"R225100845"
],
"document_role": "eln_report",
"payload": {
"aim": "To develop product equivalent to reference product",
"eln_form": {
"journal_version": "v2.0",
"equipment": "Glass RBF with stirrer set up"
},
"materials": [
{
"sr_no": 1,
"name": "Vicaspin LUB 1010 (R225100845) Bu- EO-PO HV-62.3/ MW-900",
"source": "Viswaat",
"quantity": 170.0,
"unit": "gms",
"purity_pct": 900,
"moles": 0.19,
"molar_ratio": 1.0
},
{
"sr_no": 2,
"name": "P2O5",
"source": "Commercial",
"quantity": 7.655,
"unit": "gms",
"moles": 0.054,
"molar_ratio": 0.28
},
{
"sr_no": 3,
"name": "Epomine SP-012",
"source": "Nippon",
"quantity": 37.3,
"unit": "gms",
"purity_pct": 100
},
{
"sr_no": 4,
"name": "2 ethyl hexyl acrylate",
"quantity": 59.5,
"unit": "gms",
"purity_pct": 100,
"molecular_wt": 184.3,
"moles": 0.32
},
{
"sr_no": 5,
"name": "AIBN",
"quantity": 0.79,
"unit": "gms"
},
{
"sr_no": 6,
"name": "Step- B reaction mass (20%)",
"quantity": 38.2,
"unit": "gms"
},
{
"sr_no": 7,
"name": "Step- A product",
"quantity": 164.9,
"unit": "gms"
}
],
"conditions": {
"temperature": "60-65",
"atmosphere": "N2",
"time": "4h"
},
"process_steps": [
{
"step_id": "Step- A",
"time": "0.5",
"temperature": "50-55",
"procedure": [
{
"action": "To main reactor added Vicaspin LUB 1010 (R225100845) Bu- EO-PO HV-62.3/ MW-900 under stirring and nitrogen atmosphere temp. 40 deg increased temp slowly with addition of P2O5"
}
],
"remarks": "viscous clear mass",
"step": 1
},
{
"step_id": "Step-B",
"time": "3",
"temperature": "45-50",
"procedure": [
{
"action": "To main reactor added Epomine SP-012- reaction mass held with slow addition of 2 ethyl hexyl acrylate, checked free acid at interval"
}
],
"remarks": "AV-45.0, free acid 0.5",
"step": 2
},
{
"step_id": "Step-C",
"time": "1-2",
"temperature": "65-70",
"procedure": [
{
"action": "To main reactor added Step- B reaction mass (20%) and Step- A product, mixed till uniform"
}
],
"remarks": "AV 43.2 Amine 30.0",
"step": 3
}
],
"critical_process_parameters": [
{
"sr_no": 1,
"source": "Step-A",
"time": 0.5,
"temp": 55,
"observation_details": "viscous clear mass"
},
{
"sr_no": 2,
"source": "Step-B",
"time": 3,
"temp": 60,
"observation_details": "free acid < 0.5 endpoint check"
}
],
"critical_parameters": [
{
"s_no": 1,
"parameter": "av",
"reference_value": 43.2,
"value": 43.2
},
{
"s_no": 2,
"parameter": "aminev",
"reference_value": 30.1,
"value": 30.0
}
]
},
"field_confidence": {
"aim": "high",
"materials": "high",
"conditions": "high",
"process_steps": "high",
"critical_process_parameters": "high",
"critical_parameters": "high"
},
"notes": "Conclusion section is empty in the source document. No outcome status inferred.",
"extractor_version": "direct-v1",
"extracted_date": "2026-08-27"
}